1-Amino-9-benzyliden-6,7,8,9-tetrahydro-5H-cycloheptapyridinium-mesitylensulfonat

Base Information

• Chemical Name: 1-Amino-9-benzyliden-6,7,8,9-tetrahydro-5H-cycloheptapyridinium-mesitylensulfonat
• CAS No.: 111113-98-5
• Molecular Formula: C₉H₁₁O₃S*C₁₇H₁₉N₂
• Molecular Weight: 450.602

Synonyms:1-Amino-9-benzyliden-6,7,8,9-tetrahydro-5H-cycloheptapyridinium-mesitylensulfonat

Chemical Property of 1-Amino-9-benzyliden-6,7,8,9-tetrahydro-5H-cycloheptapyridinium-mesitylensulfonat

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Technology Process of 1-Amino-9-benzyliden-6,7,8,9-tetrahydro-5H-cycloheptapyridinium-mesitylensulfonat

There total 1 articles about 1-Amino-9-benzyliden-6,7,8,9-tetrahydro-5H-cycloheptapyridinium-mesitylensulfonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

mesitylenesulfonylhydroxylamine (36016-40-7) + 9-benzylidene-6,7,8,9-tetrahydro-5H-cyclohepta[b]pyridine (89691-10-1) → 1-Amino-9-benzyliden-6,7,8,9-tetrahydro-5H-cycloheptapyridinium-mesitylensulfonat (111113-98-5)

Guidance literature:

In dichloromethane; for 1h; Ambient temperature;

Reference yield: 85.0%

chloroformic acid ethyl ester (541-41-3) + 1-Amino-9-benzyliden-6,7,8,9-tetrahydro-5H-cycloheptapyridinium-mesitylensulfonat (111113-98-5) → 9-Benzyliden-6,7,8,9-tetrahydro-5H-cycloheptapyridinium-1-(ethoxycarbonylaminid) (111113-92-9)

Guidance literature:

With potassium hydroxide; In ethanol; for 12h; Ambient temperature;

upstream raw materials:

mesitylenesulfonylhydroxylamine

9-benzylidene-6,7,8,9-tetrahydro-5H-cyclohepta[b]pyridine

Downstream raw materials:

9-Benzyliden-6,7,8,9-tetrahydro-5H-cycloheptapyridinium-1-(ethoxycarbonylaminid)

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