N-[(3S)-2-oxo-1-(pent-4-en-1-yl)azetidin-3-yl]-N-(pent-4-en-1-yl)-2-phenoxyacetamide

Base Information

Chemical Name:N-[(3S)-2-oxo-1-(pent-4-en-1-yl)azetidin-3-yl]-N-(pent-4-en-1-yl)-2-phenoxyacetamide
CAS No.:1359659-11-2
Molecular Formula:C₂₁H₂₈N₂O₃
Molecular Weight:356.465
Hs Code.:

Synonyms:N-[(3S)-2-oxo-1-(pent-4-en-1-yl)azetidin-3-yl]-N-(pent-4-en-1-yl)-2-phenoxyacetamide

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Chemical Property of N-[(3S)-2-oxo-1-(pent-4-en-1-yl)azetidin-3-yl]-N-(pent-4-en-1-yl)-2-phenoxyacetamide

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Technology Process of N-[(3S)-2-oxo-1-(pent-4-en-1-yl)azetidin-3-yl]-N-(pent-4-en-1-yl)-2-phenoxyacetamide

There total 4 articles about N-[(3S)-2-oxo-1-(pent-4-en-1-yl)azetidin-3-yl]-N-(pent-4-en-1-yl)-2-phenoxyacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1104761-72-9
(2S)-3-hydroxy-2-(2-phenoxyacetamido)propanoic acid

: 1359659-11-2
N-[(3S)-2-oxo-1-(pent-4-en-1-yl)azetidin-3-yl]-N-(pent-4-en-1-yl)-2-phenoxyacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: dicyclohexyl-carbodiimide / tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere

2: triethylamine; triphenylphosphine / tetrachloromethane; acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere

3: hydrogen / methanol; water; ethyl acetate / 12 h / 20 °C / 760.05 Torr

4: sodium hydride / N,N-dimethyl-formamide; mineral oil / 12 h / 0 - 20 °C / Inert atmosphere

With hydrogen; sodium hydride; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran; methanol; tetrachloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1002/asia.201100732

Reference yield:

: 1359659-07-6
(2S)-N-(benzyloxy)-3-hydroxy-2-(2-phenoxyacetamido)propanamide

: 1359659-11-2
N-[(3S)-2-oxo-1-(pent-4-en-1-yl)azetidin-3-yl]-N-(pent-4-en-1-yl)-2-phenoxyacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; triphenylphosphine / tetrachloromethane; acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere

2: hydrogen / methanol; water; ethyl acetate / 12 h / 20 °C / 760.05 Torr

3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 12 h / 0 - 20 °C / Inert atmosphere

With hydrogen; sodium hydride; triethylamine; triphenylphosphine; In methanol; tetrachloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1002/asia.201100732

Reference yield:

: 1359659-08-7
N-[(3S)-1-(benzyloxy)-2-oxoazetidin-3-yl]-2-phenoxyacetamide

: 1359659-11-2
N-[(3S)-2-oxo-1-(pent-4-en-1-yl)azetidin-3-yl]-N-(pent-4-en-1-yl)-2-phenoxyacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / methanol; water; ethyl acetate / 12 h / 20 °C / 760.05 Torr

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 12 h / 0 - 20 °C / Inert atmosphere

With hydrogen; sodium hydride; In methanol; water; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/asia.201100732