N-(phenyloxycarbonyl)-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

Base Information

Chemical Name:N-(phenyloxycarbonyl)-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate
CAS No.:1097200-60-6
Molecular Formula:C₂₅H₂₄NO₄P
Molecular Weight:433.444
Hs Code.:

Synonyms:N-(phenyloxycarbonyl)-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

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Chemical Property of N-(phenyloxycarbonyl)-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

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Technology Process of N-(phenyloxycarbonyl)-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

There total 1 articles about N-(phenyloxycarbonyl)-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 24923-24-8
N-(phenyloxycarbonyl)-2-oxo-azepane

: 1499-21-4
Diphenylphosphinic chloride

: 1097200-60-6
N-(phenyloxycarbonyl)-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

Guidance literature:: N-(phenyloxycarbonyl)-2-oxo-azepane; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

Diphenylphosphinic chloride; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1039/b809577a

Reference yield: 82.0%

: 1097200-60-6
N-(phenyloxycarbonyl)-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

: 172975-69-8
3,5-dimethylphenyl boronic acid

: 1097200-69-5
N-phenyloxycarbonyl-2-(3',5'-dimethylphenyl)-4,5,6,7-tetrahydro-azepane

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; In 1,2-dimethoxyethane; water; at 85 ℃; Inert atmosphere;
DOI:10.1039/b809577a

Reference yield: 81.0%

: 1097200-60-6
N-(phenyloxycarbonyl)-4,5,6,7-tetrahydro-1H-azepin-2-yl diphenylphosphinate

: 5720-07-0
4-methoxyphenylboronic acid

: 1097200-70-8
N-phenyloxycarbonyl-2-(4'-methoxyphenyl)-4,5,6,7-tetrahydro-azepane

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; In 1,2-dimethoxyethane; water; at 85 ℃; Inert atmosphere;
DOI:10.1039/b809577a