Pt(C₄H₁₄N₃)Cl₂⁽¹⁺⁾*Cl^(1-)=[Pt(C₄H₁₄N₃)Cl₂]Cl

Base Information

• Chemical Name: Pt(C₄H₁₄N₃)Cl₂⁽¹⁺⁾*Cl^(1-)=[Pt(C₄H₁₄N₃)Cl₂]Cl
• CAS No.: 108804-12-2
• Molecular Formula: C₄H₁₄Cl₂N₃Pt*Cl
• Molecular Weight: 405.614
• Mol file: 108804-12-2.mol

Synonyms:Pt(C₄H₁₄N₃)Cl₂⁽¹⁺⁾*Cl^(1-)=[Pt(C₄H₁₄N₃)Cl₂]Cl

Chemical Property of Pt(C₄H₁₄N₃)Cl₂⁽¹⁺⁾*Cl^(1-)=[Pt(C₄H₁₄N₃)Cl₂]Cl

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of Pt(C₄H₁₄N₃)Cl₂⁽¹⁺⁾*Cl^(1-)=[Pt(C₄H₁₄N₃)Cl₂]Cl

There total 1 articles about Pt(C₄H₁₄N₃)Cl₂⁽¹⁺⁾*Cl^(1-)=[Pt(C₄H₁₄N₃)Cl₂]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethylenetriamine dihydrochloride (3488-89-9,3488-90-2,4109-20-0,21120-99-0,71196-21-9) + platinum(II) chloride (10025-65-7) → Pt(C4H14N3)Cl2(1+)*Cl(1-)=[Pt(C4H14N3)Cl2]Cl (108804-12-2)

Guidance literature:

With HCl; LiOH; In water; refluxing PtCl2 in aq. HCl (overnight), filtration, addn. of dien*3HCl,addn. of LiOH to pH=3, refluxing (3 days); filtration, partial evapn., cooling in ice, recrystn. (1M HCl); elem. anal.;

DOI:10.1016/S0020-1693(00)82121-0

Reference yield: 63.0%

hydrogenchloride (7647-01-0,15364-23-5) + [Pt(diethylenetriamine*HCl)Cl2] (108804-12-2) → chloro[diethylenetriamine]platinum(II) chloride (120325-84-0,14215-58-8)

Guidance literature:

With lithium hydroxide; In water; Inorg. Chim. Acta 1987, 127, 203; platinum complex dissolved in H2O; pH adjusted to 10 with LiOH; heated (80°C, 30 min, pH kept at 10 with LiOH); cooled; pH adjusted to 4 with HCl; concd.; cooled; ppt. washed with ethanol and ether; elem. anal.;

DOI:10.1002/ejic.200500663

Reference yield:

Pt(C4H14N3)Cl2(1+)*Cl(1-)=[Pt(C4H14N3)Cl2]Cl (108804-12-2) → chloro[diethylenetriamine]platinum(II) chloride (120325-84-0,14215-58-8)

Guidance literature:

With HCl; LiOH; In water; 80°C, 30 min, pH=10 (adjustment with LiOH); cooling, pH adjustment to 4 (HCl), partial evapn., cooling in ice (crystn.), washing (EtOH, Et2O); elem. anal.;

DOI:10.1016/S0020-1693(00)82121-0

upstream raw materials:

diethylenetriamine dihydrochloride

platinum(II) chloride

Downstream raw materials:

chloro[diethylenetriamine]platinum(II) chloride

chloro(diethylenetriamine)platinum(II)