(1'S)-6,7-dimethoxy-2-2'-hydroxy-1'-phenylethyl-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:(1'S)-6,7-dimethoxy-2-2'-hydroxy-1'-phenylethyl-1,2,3,4-tetrahydroisoquinoline
CAS No.:153073-85-9
Molecular Formula:C₁₉H₂₃NO₃
Molecular Weight:313.397
Hs Code.:

Synonyms:(1'S)-6,7-dimethoxy-2-2'-hydroxy-1'-phenylethyl-1,2,3,4-tetrahydroisoquinoline

Suppliers and Price of (1'S)-6,7-dimethoxy-2-2'-hydroxy-1'-phenylethyl-1,2,3,4-tetrahydroisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1'S)-6,7-dimethoxy-2-2'-hydroxy-1'-phenylethyl-1,2,3,4-tetrahydroisoquinoline

Chemical Property:

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Technology Process of (1'S)-6,7-dimethoxy-2-2'-hydroxy-1'-phenylethyl-1,2,3,4-tetrahydroisoquinoline

There total 1 articles about (1'S)-6,7-dimethoxy-2-2'-hydroxy-1'-phenylethyl-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1745-07-9
6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

: 20780-53-4
(R)-Styrene oxide

: 153073-84-8
(2'R)-6,7-dimethoxy-2-2'-hydroxy-2'-phenylethyl-1,2,3,4-tetrahydroisoquinoline

: 153073-85-9
(1'S)-6,7-dimethoxy-2-2'-hydroxy-1'-phenylethyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: In methanol; at 100 ℃; for 20h; Yield given. Yields of byproduct given;

Reference yield: 95.0%

: 153073-85-9
(1'S)-6,7-dimethoxy-2-2'-hydroxy-1'-phenylethyl-1,2,3,4-tetrahydroisoquinoline

: (1'S)-6,7-dimethoxy-2-2'-hydroxy-1'-phenylethyl-1,2,3,4-tetrahydroisoquinoline N-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 153073-85-9
(1'S)-6,7-dimethoxy-2-2'-hydroxy-1'-phenylethyl-1,2,3,4-tetrahydroisoquinoline

: 123284-47-9
(3S,10bR)-8,9-dimethoxy-3-phenyl-2,3,5,6-tetrahydro-10bH-oxazolo<2.3-a>isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 80percent m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 0 °C

2: 100 percent / BuLi / tetrahydrofuran / 5 h / 0 - 20 °C

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;