13-cyclohexyl-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid 10-methyl ester

Base Information

Chemical Name:13-cyclohexyl-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid 10-methyl ester
CAS No.:877271-86-8
Molecular Formula:C₂₆H₂₇NO₄
Molecular Weight:417.505
Hs Code.:

Synonyms:13-cyclohexyl-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid 10-methyl ester

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Chemical Property of 13-cyclohexyl-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid 10-methyl ester

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Technology Process of 13-cyclohexyl-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid 10-methyl ester

There total 1 articles about 13-cyclohexyl-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid 10-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 877271-71-1
methyl 13-cyclohexyl-6-(carboxy)-5H-indolo[2,1-a][2]-benzazepine-10-carboxylate

: 877271-86-8
13-cyclohexyl-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid 10-methyl ester

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol; at 22 ℃; for 18 - 72h; Product distribution / selectivity;

Reference yield: 86.0%

: 110-91-8,99108-56-2
morpholine

: 877271-86-8
13-cyclohexyl-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid 10-methyl ester

: methyl 13-cyclohexyl-6,7-dihydro-6-(morpholin-4-ylcarbonyl)-5H-indolo[2,1-a][2]benzazepine-10-carboxylate

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In DMF (N,N-dimethyl-formamide); at 22 ℃; for 18h;

Reference yield: 52.0%

: 877271-86-8
13-cyclohexyl-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid 10-methyl ester

: methyl (+/-)-13-cyclohexyl-6,7-dihydro-6-hydroxymethyl-5H-indolo[2,1-a][2]benzazepine-10-carboxylate

Guidance literature:: 13-cyclohexyl-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-6,10-dicarboxylic acid 10-methyl ester; With borane-THF; In tetrahydrofuran; at 0 - 20 ℃; for 18h;

With hydrogenchloride; In tetrahydrofuran; ethyl acetate;