2-Methyl-acrylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

Base Information

Chemical Name:2-Methyl-acrylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester
CAS No.:179486-18-1
Molecular Formula:C₂₇H₃₆N₂O₄
Molecular Weight:452.594
Hs Code.:

Synonyms:2-Methyl-acrylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

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Chemical Property of 2-Methyl-acrylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

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Technology Process of 2-Methyl-acrylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

There total 3 articles about 2-Methyl-acrylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.6%

: 179486-14-7
4-[4-(11-Hydroxy-undecyloxy)-phenylazo]-phenol

: 920-46-7,26937-45-1
Methacryloyl chloride

: 179486-18-1
2-Methyl-acrylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

Guidance literature:: With pyridine; In tetrahydrofuran; for 24h; Ambient temperature;
DOI:10.1246/bcsj.69.2123

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 179486-18-1
2-Methyl-acrylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 31 percent / KOH

2: 29.8 percent / KOH, NaI / ethanol / 24 h / Heating

3: 46.6 percent / Py / tetrahydrofuran / 24 h / Ambient temperature

With pyridine; potassium hydroxide; sodium iodide; In tetrahydrofuran; ethanol;
DOI:10.1246/bcsj.69.2123

Reference yield:

: 2050-16-0
4,4'-dihydroxyazobenzene

: 179486-18-1
2-Methyl-acrylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 29.8 percent / KOH, NaI / ethanol / 24 h / Heating

2: 46.6 percent / Py / tetrahydrofuran / 24 h / Ambient temperature

With pyridine; potassium hydroxide; sodium iodide; In tetrahydrofuran; ethanol;
DOI:10.1246/bcsj.69.2123