3-12-00-03309 (Beilstein Handbook Reference)

Base Information

Chemical Name:3-12-00-03309 (Beilstein Handbook Reference)
CAS No.:93535-04-7
Molecular Formula:C₁₄H₁₂ClN
Molecular Weight:229.709
Hs Code.:
DSSTox Substance ID:DTXSID801024493
Mol file:93535-04-7.mol

Synonyms:93535-04-7;4-[2-(3-Chlorophenyl)ethenyl]benzenamine;DTXSID801024493

Suppliers and Price of 3-12-00-03309 (Beilstein Handbook Reference)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-AMINO-3'-CHLOROSTILBENE 95.00%
5MG
$ 504.33

Total 3 raw suppliers

Chemical Property of 3-12-00-03309 (Beilstein Handbook Reference)

Chemical Property:

Vapor Pressure:1.53E-06mmHg at 25°C
Boiling Point:397.9°C at 760 mmHg
Flash Point:194.5°C
PSA：26.02000
Density:1.229g/cm³
LogP:4.67380
XLogP3:4.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:229.0658271
Heavy Atom Count:16
Complexity:231

Purity/Quality:: 4-AMINO-3'-CHLOROSTILBENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)Cl)C=CC2=CC=C(C=C2)N

Technology Process of 3-12-00-03309 (Beilstein Handbook Reference)

There total 8 articles about 3-12-00-03309 (Beilstein Handbook Reference) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 51751-39-4
4-Nitro-3'-chlor-stilben

: C₁₄H₁₂ClN

: 93535-04-7,7389-20-0
(E)-4-(3-chlorostyryl)aniline

Guidance literature:: With hydrogenchloride; iron; In ethanol; water; for 4h; Reflux;
DOI:10.1016/j.ejmech.2015.05.034

Reference yield:

: 7297-53-2
(E)-3-Chloro-4'-nitrostilbene

: 93535-04-7,7389-20-0
(E)-4-(3-chlorostyryl)aniline

Guidance literature:: With acetic acid; tin(ll) chloride;

Reference yield:

: 2039-85-2,26100-04-9
3-Chlorostyrene

: 106-40-1
4-bromo-aniline

: 1370449-53-8
C₁₄H₁₂ClN

: 93535-04-7,7389-20-0
(E)-4-(3-chlorostyryl)aniline

Guidance literature:: With dichloro{bis[1-(dicyclohexylphosphanyl)piperidine]}palladium; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; at 140 ℃; for 8h; Inert atmosphere;
DOI:10.1002/adsc.201100646