Acetic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-5,6-dihydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Base Information

• Chemical Name: Acetic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-5,6-dihydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester
• CAS No.: 123285-93-8
• Molecular Formula: C₂₉H₅₀O₄
• Molecular Weight: 462.714

Synonyms:Acetic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-5,6-dihydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Chemical Property of Acetic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-5,6-dihydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Chemical Property:

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Technology Process of Acetic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-5,6-dihydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

There total 1 articles about Acetic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-5,6-dihydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Cholesteryl acetate (604-35-3) → cholestanetriol (1253-84-5) + 3β,5-dihydroxy-5α-cholestan-6-one (2953-37-9,6580-08-1,16526-63-9,97100-50-0,115792-36-4,13027-33-3) + 3β-acetoxycholestane-5α,6β-diol (2701-08-8,35089-26-0,98076-44-9,117465-73-3,123285-93-8,1857-99-4) + 3β-acetoxy-5α-hydroxycholestan-6-one (6580-09-2,14956-13-9,60803-77-2,96478-98-7,1258-38-4) + 5α-bromo-6-ketocholestan-3β-yl acetate (14956-20-8) + 6α-bromo-5β-hydroxy-cholestan-3β-yl acetate (117141-97-6)

Guidance literature:

With N-Bromosuccinimide; In dimethyl sulfoxide; for 312h; Mechanism; Ambient temperature;

Reference yield: 94.0%

Acetic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-5,6-dihydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (123285-93-8) → 3β-acetoxy-5-oxo-5,6-seco-cholestan-6-oic acid (10473-42-4)

Guidance literature:

With jones reagent; In acetone; at 50 ℃;

DOI:10.1016/S0040-4039(00)82357-6

Reference yield: 93.0%

3β-acetoxycholestane-5α,6β-diol (2701-08-8,35089-26-0,98076-44-9,117465-73-3,123285-93-8,1857-99-4) + p-toluenesulfonyl chloride (98-59-9) → 3β-acetoxy-5α-cholestane-5,6β-diol 6-toluene-p-sulfonate (33346-99-5,72342-03-1)

Guidance literature:

In pyridine; for 48h; Ambient temperature;

upstream raw materials:

Cholesteryl acetate

Downstream raw materials:

3β-acetoxy-5α-cholestane-5,6β-diol 6-toluene-p-sulfonate

3-Methoxy-benzoic acid (3S,5R,6R,8S,9S,10R,13R,14S,17R)-3-acetoxy-17-((R)-1,5-dimethyl-hexyl)-5-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-6-yl ester

5α-Cholestan-3β,5,6β-triol-3-acetat-6-benzoat

4-Chloro-benzoic acid (3S,5R,6R,8S,9S,10R,13R,14S,17R)-3-acetoxy-17-((R)-1,5-dimethyl-hexyl)-5-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-6-yl ester

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