4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-5-oxo-2-phenyl-1H-imidazol-1-yl>benzoic acid hydrazide

Base Information

• Chemical Name: 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-5-oxo-2-phenyl-1H-imidazol-1-yl>benzoic acid hydrazide
• CAS No.: 134248-34-3
• Molecular Formula: C₂₅H₁₉N₅O₂
• Molecular Weight: 421.458

Synonyms:4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-5-oxo-2-phenyl-1H-imidazol-1-yl>benzoic acid hydrazide

Chemical Property of 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-5-oxo-2-phenyl-1H-imidazol-1-yl>benzoic acid hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-5-oxo-2-phenyl-1H-imidazol-1-yl>benzoic acid hydrazide

There total 3 articles about 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-5-oxo-2-phenyl-1H-imidazol-1-yl>benzoic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-5-oxo-2-phenyl-1H-imidazol-1-yl>benzoate (134248-30-9) → 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-5-oxo-2-phenyl-1H-imidazol-1-yl>benzoic acid hydrazide (134248-34-3)

Guidance literature:

With hydrazine hydrate; In ethanol; for 8h; Heating;

Reference yield:

for 3e (42136-84-5,102913-26-8) → 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-5-oxo-2-phenyl-1H-imidazol-1-yl>benzoic acid hydrazide (134248-34-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / 0.33 h / 140 °C

2: 78 percent / 99percent N₂H₄*H₂O / ethanol / 8 h / Heating

With hydrazine hydrate; In ethanol;

Reference yield:

4-methoxycarbonyl aniline (619-45-4) → 4-<4,5-Dihydro-4-(1H-indol-3-ylmethylene)-5-oxo-2-phenyl-1H-imidazol-1-yl>benzoic acid hydrazide (134248-34-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / 0.33 h / 140 °C

2: 78 percent / 99percent N₂H₄*H₂O / ethanol / 8 h / Heating

With hydrazine hydrate; In ethanol;

upstream raw materials:

Methyl 4-<4,5-dihydro-4-(1H-indol-3-ylmethylene)-5-oxo-2-phenyl-1H-imidazol-1-yl>benzoate

for 3e

4-methoxycarbonyl aniline

Downstream raw materials:

4-{4-[1-(1H-Indol-3-yl)-meth-(Z)-ylidene]-5-oxo-2-phenyl-4,5-dihydro-imidazol-1-yl}-benzoic acid [1-(3,4-dimethoxy-phenyl)-meth-(Z)-ylidene]-hydrazide

4-{4-[1-(1H-Indol-3-yl)-meth-(Z)-ylidene]-5-oxo-2-phenyl-4,5-dihydro-imidazol-1-yl}-benzoic acid [1-(4-chloro-phenylazo)-1-(3,4-dimethoxy-phenyl)-meth-(E)-ylidene]-hydrazide

4-{4-[1-(1H-Indol-3-yl)-meth-(Z)-ylidene]-5-oxo-2-phenyl-4,5-dihydro-imidazol-1-yl}-benzoic acid [1-(3,4-dimethoxy-phenyl)-1-o-tolylazo-meth-(E)-ylidene]-hydrazide

4-{4-[1-(1H-Indol-3-yl)-meth-(Z)-ylidene]-5-oxo-2-phenyl-4,5-dihydro-imidazol-1-yl}-benzoic acid [1-(4-chloro-phenylazo)-1-(2-hydroxy-phenyl)-meth-(E)-ylidene]-hydrazide

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