3-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-3-oxopropionic acid methyl ester

Base Information

Chemical Name:3-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-3-oxopropionic acid methyl ester
CAS No.:308277-48-7
Molecular Formula:C₁₄H₁₇NO₅
Molecular Weight:279.293
Hs Code.:

Synonyms:3-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-3-oxopropionic acid methyl ester

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Chemical Property of 3-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-3-oxopropionic acid methyl ester

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Technology Process of 3-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-3-oxopropionic acid methyl ester

There total 3 articles about 3-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-3-oxopropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 37517-81-0
3-chloro-3-oxopropanoic acid methyl ester

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 308277-48-7
3-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-3-oxopropionic acid methyl ester

Guidance literature:: methyl (2S)-2-amino-3-phenylpropanoate hydrochloride; With sodium hydrogencarbonate; In dichloromethane; water; at 23 ℃;

3-chloro-3-oxopropanoic acid methyl ester; In dichloromethane; water; at 23 ℃;
DOI:10.15227/orgsyn.096.0528

Reference yield: 97.0%

: 37517-81-0
3-chloro-3-oxopropanoic acid methyl ester

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 308277-48-7
3-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-3-oxopropionic acid methyl ester

Guidance literature:: With 4-methyl-morpholine; In dichloromethane; at -15 - 20 ℃; for 12h;
DOI:10.1002/1099-0690(200009)2000:18<3217::AID-EJOC3217>3.0.CO;2-#

Reference yield: 85.0%

: 16695-14-0
Malonic acid monomethyl ester

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 308277-48-7
3-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-3-oxopropionic acid methyl ester

Guidance literature:: Malonic acid monomethyl ester; methyl (2S)-2-amino-3-phenylpropanoate hydrochloride; With dmap; triethylamine; In dichloromethane; for 0.5h; Cooling with ice;

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;