2,2'-(((2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(oxy))dibenzaldehyde

Base Information

Chemical Name:2,2'-(((2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(oxy))dibenzaldehyde
CAS No.:1429743-92-9
Molecular Formula:C₂₅H₂₄O₄
Molecular Weight:388.463
Hs Code.:

Synonyms:2,2'-(((2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(oxy))dibenzaldehyde

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Chemical Property of 2,2'-(((2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(oxy))dibenzaldehyde

Chemical Property:

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Technology Process of 2,2'-(((2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(oxy))dibenzaldehyde

There total 2 articles about 2,2'-(((2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(oxy))dibenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 90-02-8
salicylaldehyde

: 55231-61-3
2,4-bis(bromomethyl)-1,3,5-trimethylbenzene

: 1429743-92-9
2,2'-(((2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(oxy))dibenzaldehyde

Guidance literature:: salicylaldehyde; With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In acetonitrile; for 0.333333h; Reflux;

2,4-bis(bromomethyl)-1,3,5-trimethylbenzene; In acetonitrile; for 8h; Reflux;
DOI:10.1039/c3nj01086d

Reference yield:

: 108-67-8
1,3,5-trimethyl-benzene

: 1429743-92-9
2,2'-(((2,4,6-trimethyl-1,3-phenylene)bis(methylene))bis(oxy))dibenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide; acetic acid / 15 h / Reflux

2: tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / acetonitrile / 15 h / Reflux

With hydrogen bromide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; acetic acid; In acetonitrile;
DOI:10.1002/ejic.201402473