(2,6-dimethoxy-1-methylcyclohexa-2,5-dienyl)(dimethyl)phenylsilane

Base Information

• Chemical Name: (2,6-dimethoxy-1-methylcyclohexa-2,5-dienyl)(dimethyl)phenylsilane
• CAS No.: 356070-10-5
• Molecular Formula: C₁₇H₂₄O₂Si
• Molecular Weight: 288.462
• Mol file: 356070-10-5.mol

Synonyms:(2,6-dimethoxy-1-methylcyclohexa-2,5-dienyl)(dimethyl)phenylsilane

Chemical Property of (2,6-dimethoxy-1-methylcyclohexa-2,5-dienyl)(dimethyl)phenylsilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2,6-dimethoxy-1-methylcyclohexa-2,5-dienyl)(dimethyl)phenylsilane

There total 1 articles about (2,6-dimethoxy-1-methylcyclohexa-2,5-dienyl)(dimethyl)phenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

1,5-dimethoxy-1,4-cyclohexadiene (37567-78-5) + phenyldimethylsilyl chloride (768-33-2) + dimethyl sulfate (77-78-1) → (2,6-dimethoxy-1-methylcyclohexa-2,5-dienyl)(dimethyl)phenylsilane (356070-10-5)

Guidance literature:

Multistep reaction;

DOI:10.1002/1522-2675(200210)85:10<3559::AID-HLCA3559>3.0.CO;2-6

Reference yield: 57.0%

dimethyl bisallylmalonate (35357-77-8) + (2,6-dimethoxy-1-methylcyclohexa-2,5-dienyl)(dimethyl)phenylsilane (356070-10-5) → 3-[(dimethyl-phenyl-silanyl)-methyl]-4-methyl-cyclopentane-1,1-dicarboxylic acid dimethyl ester

Guidance literature:

With azobisisobutyronitrile; In hexane;

DOI:10.1002/1522-2675(200210)85:10<3559::AID-HLCA3559>3.0.CO;2-6

Reference yield: 34.0%

phenylacetylene (536-74-3) + (2,6-dimethoxy-1-methylcyclohexa-2,5-dienyl)(dimethyl)phenylsilane (356070-10-5) → dimethyl(phenyl)[2-phenylethenyl]silane (128756-74-1)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In hexane; at 80 - 85 ℃;

DOI:10.1002/1522-2675(200210)85:10<3559::AID-HLCA3559>3.0.CO;2-6

upstream raw materials:

1,5-dimethoxy-1,4-cyclohexadiene

phenyldimethylsilyl chloride

dimethyl sulfate

Downstream raw materials:

(E)-4-[dimethyl(phenyl)silyl]but-2-en-1-ol

dimethyl(phenyl)[2-phenylethenyl]silane

dimethyl(hex-1-enyl)(phenyl)silane