N-(2,4-dimethylphenyl)-4-(1-hydroxy-2-((pyridin-3-ylmethyl)amino)ethyl)-N-isobutylbenzenesulfonamide

Base Information

Chemical Name:N-(2,4-dimethylphenyl)-4-(1-hydroxy-2-((pyridin-3-ylmethyl)amino)ethyl)-N-isobutylbenzenesulfonamide
CAS No.:1429347-01-2
Molecular Formula:C₂₆H₃₃N₃O₃S
Molecular Weight:467.632
Hs Code.:

Synonyms:N-(2,4-dimethylphenyl)-4-(1-hydroxy-2-((pyridin-3-ylmethyl)amino)ethyl)-N-isobutylbenzenesulfonamide

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Chemical Property of N-(2,4-dimethylphenyl)-4-(1-hydroxy-2-((pyridin-3-ylmethyl)amino)ethyl)-N-isobutylbenzenesulfonamide

Chemical Property:

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Technology Process of N-(2,4-dimethylphenyl)-4-(1-hydroxy-2-((pyridin-3-ylmethyl)amino)ethyl)-N-isobutylbenzenesulfonamide

There total 3 articles about N-(2,4-dimethylphenyl)-4-(1-hydroxy-2-((pyridin-3-ylmethyl)amino)ethyl)-N-isobutylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3731-52-0
3-Aminomethylpyridine

: 1429347-55-6
N-(2,4-dimethylphenyl)-N-isobutyl-4-(oxiran-2-yl)benzenesulfonamide

: 1429347-01-2
N-(2,4-dimethylphenyl)-4-(1-hydroxy-2-((pyridin-3-ylmethyl)amino)ethyl)-N-isobutylbenzenesulfonamide

Guidance literature:: With triethylamine; In ethanol; at 40 - 50 ℃;

Reference yield:

: 1429346-28-0
4-bromo-N-(2,4-dimethylphenyl)-N-isobutylbenzenesulfonamide

: 1429347-01-2
N-(2,4-dimethylphenyl)-4-(1-hydroxy-2-((pyridin-3-ylmethyl)amino)ethyl)-N-isobutylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; caesium carbonate; palladium dichloride / water; tetrahydrofuran / 1.5 h / 140 °C / Microwave irradiation

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 25 °C

3: triethylamine / ethanol / 40 - 50 °C

With caesium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; palladium dichloride; In tetrahydrofuran; ethanol; dichloromethane; water;

Reference yield:

: 1429347-54-5
N-(2,4-dimethylphenyl)-N-isobutyl-4-vinylbenzenesulfonamide

: 1429347-01-2
N-(2,4-dimethylphenyl)-4-(1-hydroxy-2-((pyridin-3-ylmethyl)amino)ethyl)-N-isobutylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 25 °C

2: triethylamine / ethanol / 40 - 50 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane;