C₅₅H₁₀₀O₉Si₃

Base Information

Chemical Name:C₅₅H₁₀₀O₉Si₃
CAS No.:1028432-83-8
Molecular Formula:C₅₅H₁₀₀O₉Si₃
Molecular Weight:989.65
Hs Code.:

C<sub>55</sub>H<sub>100</sub>O<sub>9</sub>Si<sub>3</sub>

Synonyms:C₅₅H₁₀₀O₉Si₃

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Chemical Property of C₅₅H₁₀₀O₉Si₃

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Technology Process of C₅₅H₁₀₀O₉Si₃

There total 6 articles about C₅₅H₁₀₀O₉Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1028432-81-6
C₅₆H₁₀₂O₉SSi₃

: 75-24-1
trimethylaluminum

: 1028432-83-8
C₅₅H₁₀₀O₉Si₃

Guidance literature:: C₅₆H₁₀₂O₉SSi₃; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃; for 2h; Inert atmosphere;

trimethylaluminum; In hexane; dichloromethane; at -78 - 0 ℃; for 1.33333h; Inert atmosphere;
DOI:10.1021/ol800685c

Reference yield:

: 1028433-12-6
C₃₈H₆₀O₉S

: 1028432-83-8
C₅₅H₁₀₀O₉Si₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 9.17 h / 0 - 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3.5 h / -78 °C

2.2: -78 - 0 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1002/chem.201101437

Reference yield:

: 1360873-01-3
C₆₂H₉₆O₁₁Si₂

: 1028432-83-8
C₅₅H₁₀₀O₉Si₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

3.1: hydrogenchloride / tetrahydrofuran; methanol; water / 21.5 h / 60 °C

3.2: 20 h / 20 °C

4.1: triethylamine / dichloromethane / 9.17 h / 0 - 20 °C

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3.5 h / -78 °C

5.2: -78 - 0 °C

With hydrogenchloride; tetrapropylammonium perruthennate; dimethylsulfide borane complex; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/chem.201101437