Technology Process of C29H42O7S
There total 5 articles about C29H42O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / water; tert-butyl alcohol / 80 - 90 °C
1.2: 6.5 h / 80 - 90 °C
1.3: pH 1.5
2.1: thionyl chloride / 0 °C / Inert atmosphere; Reflux
3.1: toluene-4-sulfonic acid / toluene / 5 h / Reflux
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C
5.1: pyridine / dichloromethane / 20 °C
With
pyridine; lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; toluene-4-sulfonic acid;
In
tetrahydrofuran; dichloromethane; water; toluene; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride / 0 °C / Inert atmosphere; Reflux
2: toluene-4-sulfonic acid / toluene / 5 h / Reflux
3: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C
4: pyridine / dichloromethane / 20 °C
With
pyridine; lithium aluminium tetrahydride; thionyl chloride; toluene-4-sulfonic acid;
In
tetrahydrofuran; dichloromethane; toluene;