C₄₆H₅₆N₂O₁₀Si₂

Base Information

Chemical Name:C₄₆H₅₆N₂O₁₀Si₂
CAS No.:1410805-62-7
Molecular Formula:C₄₆H₅₆N₂O₁₀Si₂
Molecular Weight:853.129
Hs Code.:

C<sub>46</sub>H<sub>56</sub>N<sub>2</sub>O<sub>10</sub>Si<sub>2</sub>

Synonyms:C₄₆H₅₆N₂O₁₀Si₂

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Chemical Property of C₄₆H₅₆N₂O₁₀Si₂

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Technology Process of C₄₆H₅₆N₂O₁₀Si₂

There total 12 articles about C₄₆H₅₆N₂O₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₆H₅₆N₂O₉Si₂

: 1410805-62-7
C₄₆H₅₆N₂O₁₀Si₂

Guidance literature:: With dimethylsulfide; oxygen; In dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/ol302691j

Reference yield:

: C₅₂H₇₄N₂O₁₀Si₃

: 1410805-62-7
C₄₆H₅₆N₂O₁₀Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: Martins sulfurane / dichloromethane / 0.5 h / -78 - 20 °C / Inert atmosphere

2: methanol / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

4: copper(II) acetate monohydrate / methanol / 22 h / 20 °C / Inert atmosphere

5: cerium(III) chloride heptahydrate / isopropyl alcohol / 1 h / 20 °C / Inert atmosphere

6: oxygen; dimethylsulfide / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

With methanol; Martins sulfurane; dimethylsulfide; cerium(III) chloride heptahydrate; oxygen; copper(II) acetate monohydrate; Dess-Martin periodane; In methanol; dichloromethane; isopropyl alcohol; 5: |Michael Addition;
DOI:10.1021/ol302691j

Reference yield:

: C₅₂H₇₃BrN₂O₁₀Si₃

: 1410805-62-7
C₄₆H₅₆N₂O₁₀Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: samarium diiodide / tetrahydrofuran / 0.42 h / -78 °C / Inert atmosphere

2: Martins sulfurane / dichloromethane / 0.5 h / -78 - 20 °C / Inert atmosphere

3: methanol / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

4: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

5: copper(II) acetate monohydrate / methanol / 22 h / 20 °C / Inert atmosphere

6: cerium(III) chloride heptahydrate / isopropyl alcohol / 1 h / 20 °C / Inert atmosphere

7: oxygen; dimethylsulfide / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

With methanol; samarium diiodide; Martins sulfurane; dimethylsulfide; cerium(III) chloride heptahydrate; oxygen; copper(II) acetate monohydrate; Dess-Martin periodane; In tetrahydrofuran; methanol; dichloromethane; isopropyl alcohol; 1: |Reformatsky Reaction / 6: |Michael Addition;
DOI:10.1021/ol302691j