Technology Process of 2,4-bis(allyloxy)-5-iodobenzaldehyde
There total 2 articles about 2,4-bis(allyloxy)-5-iodobenzaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; sodium iodide;
In
N,N-dimethyl-formamide;
at 50 ℃;
for 1h;
Inert atmosphere;
DOI:10.3762/bjoc.8.123
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Iodine monochloride; acetic acid / 5 h / 20 °C / Inert atmosphere
2: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 1 h / 50 °C / Inert atmosphere
With
Iodine monochloride; potassium carbonate; acetic acid; sodium iodide;
In
N,N-dimethyl-formamide;
DOI:10.3762/bjoc.8.123
- Guidance literature:
-
2,4-bis(allyloxy)-5-iodobenzaldehyde;
With
titanium tetrachloride; tetra-(n-butyl)ammonium iodide;
In
dichloromethane;
at 0 - 20 ℃;
for 12.5h;
Inert atmosphere;
With
hydrogenchloride; sodium hydrogen sulfate;
In
diethyl ether; dichloromethane; water;
DOI:10.3762/bjoc.8.123
