N-[(6-methoxy-2-nitrophenyl)methyl]-N-[2-(4-pyridyl)-1,3-thiazol-4-yl]-prop-2-enyloxycarboxamide

Base Information

• Chemical Name: N-[(6-methoxy-2-nitrophenyl)methyl]-N-[2-(4-pyridyl)-1,3-thiazol-4-yl]-prop-2-enyloxycarboxamide
• CAS No.: 950185-70-3
• Molecular Formula: C₂₀H₁₈N₄O₅S
• Molecular Weight: 426.453

Synonyms:N-[(6-methoxy-2-nitrophenyl)methyl]-N-[2-(4-pyridyl)-1,3-thiazol-4-yl]-prop-2-enyloxycarboxamide

Chemical Property of N-[(6-methoxy-2-nitrophenyl)methyl]-N-[2-(4-pyridyl)-1,3-thiazol-4-yl]-prop-2-enyloxycarboxamide

Chemical Property:

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Technology Process of N-[(6-methoxy-2-nitrophenyl)methyl]-N-[2-(4-pyridyl)-1,3-thiazol-4-yl]-prop-2-enyloxycarboxamide

There total 1 articles about N-[(6-methoxy-2-nitrophenyl)methyl]-N-[2-(4-pyridyl)-1,3-thiazol-4-yl]-prop-2-enyloxycarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

N-(2-pyridin-4-yl-1,3-thiazol-4-yl)prop-2-enyloxycarboxamide (630409-36-8) + 2-nitro-6-methoxybenzyl bromide (19689-86-2) → N-[(6-methoxy-2-nitrophenyl)methyl]-N-[2-(4-pyridyl)-1,3-thiazol-4-yl]-prop-2-enyloxycarboxamide (950185-70-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 80 ℃;

DOI:10.1016/j.bmc.2007.07.005

Reference yield:

N-[(6-methoxy-2-nitrophenyl)methyl]-N-[2-(4-pyridyl)-1,3-thiazol-4-yl]-prop-2-enyloxycarboxamide (950185-70-3) → [(6-methoxy-2-nitrophenyl)methyl](2-(pyridin-4-yl)(1,3-thiazol-4-yl))amine

Guidance literature:

With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In acetonitrile; at 20 ℃;

DOI:10.1016/j.bmc.2007.07.005

upstream raw materials:

N-(2-pyridin-4-yl-1,3-thiazol-4-yl)prop-2-enyloxycarboxamide

2-nitro-6-methoxybenzyl bromide

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