3,5-bis[4-{diazo(4-tert-butyl-2,6-dimethylphenyl)methyl}-3,5-bromophenylethynyl]phenylacetylene

Base Information

Chemical Name:3,5-bis[4-{diazo(4-tert-butyl-2,6-dimethylphenyl)methyl}-3,5-bromophenylethynyl]phenylacetylene
CAS No.:763110-75-4
Molecular Formula:C₅₀H₄₂Br₄N₄
Molecular Weight:1018.53
Hs Code.:

Synonyms:3,5-bis[4-{diazo(4-tert-butyl-2,6-dimethylphenyl)methyl}-3,5-bromophenylethynyl]phenylacetylene

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Chemical Property of 3,5-bis[4-{diazo(4-tert-butyl-2,6-dimethylphenyl)methyl}-3,5-bromophenylethynyl]phenylacetylene

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Technology Process of 3,5-bis[4-{diazo(4-tert-butyl-2,6-dimethylphenyl)methyl}-3,5-bromophenylethynyl]phenylacetylene

There total 1 articles about 3,5-bis[4-{diazo(4-tert-butyl-2,6-dimethylphenyl)methyl}-3,5-bromophenylethynyl]phenylacetylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 763110-74-3
(3,5-bis-{3,5-dibromo-4-[(4-tert-butyl-2,6-dimethyl-phenyl)-diazo-methyl]-phenylethynyl}-phenylethynyl)-trimethyl-silane

: 763110-75-4
3,5-bis[4-{diazo(4-tert-butyl-2,6-dimethylphenyl)methyl}-3,5-bromophenylethynyl]phenylacetylene

Guidance literature:: With potassium carbonate; In tetrahydrofuran; methanol; at 20 ℃;
DOI:10.1002/ejoc.200400123

Reference yield: 79.0%

: 626-44-8
1,3,5-Triiodobenzene

: 763110-75-4
3,5-bis[4-{diazo(4-tert-butyl-2,6-dimethylphenyl)methyl}-3,5-bromophenylethynyl]phenylacetylene

: C₁₅₆H₁₂₆Br₁₂N₁₂

Guidance literature:: With copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; In triethylamine; at 20 ℃; for 48h;
DOI:10.1002/ejoc.200400123

Reference yield: 67.0%

: 210905-25-2
2-(3,5-diiodophenyl)-1-(trimethylsilyl)acetylene

: 763110-75-4
3,5-bis[4-{diazo(4-tert-butyl-2,6-dimethylphenyl)methyl}-3,5-bromophenylethynyl]phenylacetylene

: C₁₁₁H₉₄Br₈N₈Si

Guidance literature:: With copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; In triethylamine; at 20 ℃; for 48h;
DOI:10.1002/ejoc.200400123