2-(3,5-diiodophenyl)-1-(trimethylsilyl)acetylene

Base Information

Chemical Name:2-(3,5-diiodophenyl)-1-(trimethylsilyl)acetylene
CAS No.:210905-25-2
Molecular Formula:C₁₁H₁₂I₂Si
Molecular Weight:426.111
Hs Code.:

Synonyms:2-(3,5-diiodophenyl)-1-(trimethylsilyl)acetylene

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Chemical Property of 2-(3,5-diiodophenyl)-1-(trimethylsilyl)acetylene

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Technology Process of 2-(3,5-diiodophenyl)-1-(trimethylsilyl)acetylene

There total 4 articles about 2-(3,5-diiodophenyl)-1-(trimethylsilyl)acetylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 135853-29-1
3',5'-dibromo-2-phenyl-1-(trimethylsilyl)acetylene

: 210905-25-2
2-(3,5-diiodophenyl)-1-(trimethylsilyl)acetylene

Guidance literature:: 3',5'-dibromo-2-phenyl-1-(trimethylsilyl)acetylene; With n-butyllithium; In diethyl ether; at -80 ℃;

With iodine; In diethyl ether; at -80 - 25 ℃;
DOI:10.1002/chem.200701915

Reference yield: 81.0%

: 75-77-4
chloro-trimethyl-silane

: 188348-48-3
1-ethynyl-3,5-diiodobenzene

: 210905-25-2
2-(3,5-diiodophenyl)-1-(trimethylsilyl)acetylene

Guidance literature:: 1-ethynyl-3,5-diiodobenzene; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; at -78 ℃; Inert atmosphere;
DOI:10.1021/jo9021748

Reference yield: 51.0%

: 626-44-8
1,3,5-Triiodobenzene

: 1066-54-2
trimethylsilylacetylene

: 210905-25-2
2-(3,5-diiodophenyl)-1-(trimethylsilyl)acetylene

Guidance literature:: With pyridine; copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; at 35 ℃; for 2h;
DOI:10.1021/jo980846+