diphenyl (1-benzo[b]thiophen-3-yl((6-chlorobenzo[d]thiazol-2-yl)amino)methyl)phosphonate

Base Information

• Chemical Name: diphenyl (1-benzo[b]thiophen-3-yl((6-chlorobenzo[d]thiazol-2-yl)amino)methyl)phosphonate
• CAS No.: 1582739-83-0
• Molecular Formula: C₂₈H₂₀ClN₂O₃PS₂
• Molecular Weight: 563.037

Synonyms:diphenyl (1-benzo[b]thiophen-3-yl((6-chlorobenzo[d]thiazol-2-yl)amino)methyl)phosphonate

Chemical Property of diphenyl (1-benzo[b]thiophen-3-yl((6-chlorobenzo[d]thiazol-2-yl)amino)methyl)phosphonate

Chemical Property:

Purity/Quality:

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Technology Process of diphenyl (1-benzo[b]thiophen-3-yl((6-chlorobenzo[d]thiazol-2-yl)amino)methyl)phosphonate

There total 3 articles about diphenyl (1-benzo[b]thiophen-3-yl((6-chlorobenzo[d]thiazol-2-yl)amino)methyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diphenyl hydrogen phosphite (4712-55-4) + C16H9ClN2S2 (1582739-77-2) → diphenyl (1-benzo[b]thiophen-3-yl((6-chlorobenzo[d]thiazol-2-yl)amino)methyl)phosphonate (1582739-83-0)

Guidance literature:

In toluene; at 20 ℃; for 8h; Reflux;

DOI:10.1080/10426507.2013.829837

Reference yield:

benzothiophene-3-carboxaldehyde (5381-20-4) → diphenyl (1-benzo[b]thiophen-3-yl((6-chlorobenzo[d]thiazol-2-yl)amino)methyl)phosphonate (1582739-83-0)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / toluene / 10 h / Reflux

2: toluene / 8 h / 20 °C / Reflux

With acetic acid; In toluene;

DOI:10.1080/10426507.2013.829837

Reference yield:

6-chloro-2-aminobenzothiazole (95-24-9) → diphenyl (1-benzo[b]thiophen-3-yl((6-chlorobenzo[d]thiazol-2-yl)amino)methyl)phosphonate (1582739-83-0)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid / toluene / 10 h / Reflux

2: toluene / 8 h / 20 °C / Reflux

With acetic acid; In toluene;

DOI:10.1080/10426507.2013.829837

upstream raw materials:

diphenyl hydrogen phosphite

C₁₆H₉ClN₂S₂

benzothiophene-3-carboxaldehyde

6-chloro-2-aminobenzothiazole

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