3-butyryl-4-(4-hydroxy-2-methylphenylamino)-8-(4-methoxybenzoyloxymethyl)-quinoline

Base Information

Chemical Name:3-butyryl-4-(4-hydroxy-2-methylphenylamino)-8-(4-methoxybenzoyloxymethyl)-quinoline
CAS No.:125500-47-2
Molecular Formula:C₂₉H₂₈N₂O₅
Molecular Weight:484.552
Hs Code.:

Synonyms:3-butyryl-4-(4-hydroxy-2-methylphenylamino)-8-(4-methoxybenzoyloxymethyl)-quinoline

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Chemical Property of 3-butyryl-4-(4-hydroxy-2-methylphenylamino)-8-(4-methoxybenzoyloxymethyl)-quinoline

Chemical Property:

Purity/Quality:

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Technology Process of 3-butyryl-4-(4-hydroxy-2-methylphenylamino)-8-(4-methoxybenzoyloxymethyl)-quinoline

There total 6 articles about 3-butyryl-4-(4-hydroxy-2-methylphenylamino)-8-(4-methoxybenzoyloxymethyl)-quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3249-68-1
ethyl butyroyl acetate

: 125500-47-2
3-butyryl-4-(4-hydroxy-2-methylphenylamino)-8-(4-methoxybenzoyloxymethyl)-quinoline

Guidance literature:: Multi-step reaction with 6 steps

1: Ac₂O

2: 85 percent / 0.17 h / 100 °C

3: 58 percent / pyridine / 16 h

4: 54 percent / diphenyl ether / 0.5 h / Heating

5: POCl₃ / 0.5 h / Heating

6: dioxane / Heating

With pyridine; acetic anhydride; trichlorophosphate; In 1,4-dioxane; diphenylether;
DOI:10.1021/jm00014a026

Reference yield:

: 125500-84-7
ethyl 2-(ethoxymethylene)-3-oxohexanoate

: 125500-47-2
3-butyryl-4-(4-hydroxy-2-methylphenylamino)-8-(4-methoxybenzoyloxymethyl)-quinoline

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / 0.17 h / 100 °C

2: 58 percent / pyridine / 16 h

3: 54 percent / diphenyl ether / 0.5 h / Heating

4: POCl₃ / 0.5 h / Heating

5: dioxane / Heating

With pyridine; trichlorophosphate; In 1,4-dioxane; diphenylether;
DOI:10.1021/jm00014a026

Reference yield:

: 125500-85-8
2-[1-(2-Hydroxymethyl-phenylamino)-meth-(Z)-ylidene]-3-oxo-hexanoic acid ethyl ester

: 125500-47-2
3-butyryl-4-(4-hydroxy-2-methylphenylamino)-8-(4-methoxybenzoyloxymethyl)-quinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 58 percent / pyridine / 16 h

2: 54 percent / diphenyl ether / 0.5 h / Heating

3: POCl₃ / 0.5 h / Heating

4: dioxane / Heating

With pyridine; trichlorophosphate; In 1,4-dioxane; diphenylether;
DOI:10.1021/jm00014a026