C₁₉H₂₆O₄

Base Information

Chemical Name:C₁₉H₂₆O₄
CAS No.:1313999-63-1
Molecular Formula:C₁₉H₂₆O₄
Molecular Weight:318.413
Hs Code.:

C<sub>19</sub>H<sub>26</sub>O<sub>4</sub>

Synonyms:C₁₉H₂₆O₄

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Chemical Property of C₁₉H₂₆O₄

Chemical Property:

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Technology Process of C₁₉H₂₆O₄

There total 9 articles about C₁₉H₂₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1313999-68-6
C₁₉H₂₈O₄

: 1313999-63-1
C₁₉H₂₆O₄

Guidance literature:: With manganese(IV) oxide; In toluene; for 2h; Reflux;
DOI:10.1039/c1cc11919b

Reference yield:

: 1313999-60-8
2-(2-bromo-3,5-dimethoxyphenyl)-3-tert-butyl-4,4-dimethyltetrahydrofuran-3-ol

: 1313999-63-1
C₁₉H₂₆O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine; sulfuryl dichloride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 4 h / -78 - -5 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / tetrahydrofuran / 6 h / -78 - 20 °C / Inert atmosphere

4.1: manganese(IV) oxide / toluene / 2 h / Reflux

With pyridine; manganese(IV) oxide; n-butyllithium; sulfuryl dichloride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1039/c1cc11919b

Reference yield:

: 1313999-66-4
1-(3,5-dimethoxybenzyloxy)-2,2,4,4-tetramethylpentan-3-ol

: 1313999-63-1
C₁₉H₂₆O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridinium chlorochromate / dichloromethane / 20 °C / Inert atmosphere

2.1: potassium tert-butylate / dimethyl sulfoxide / 7 h / 20 °C / Cooling; Inert atmosphere

3.1: N-Bromosuccinimide / tetrahydrofuran; water / 0 - 20 °C / Inert atmosphere

4.1: pyridine; sulfuryl dichloride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

5.2: 4 h / -78 - -5 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / tetrahydrofuran / 6 h / -78 - 20 °C / Inert atmosphere

7.1: manganese(IV) oxide / toluene / 2 h / Reflux

With pyridine; manganese(IV) oxide; N-Bromosuccinimide; n-butyllithium; sulfuryl dichloride; potassium tert-butylate; diisobutylaluminium hydride; pyridinium chlorochromate; In tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfoxide; toluene;
DOI:10.1039/c1cc11919b