methyl 4,5-dimethoxy-2-N-benzeneacetate

Base Information

Chemical Name:methyl 4,5-dimethoxy-2-N-benzeneacetate
CAS No.:118671-18-4
Molecular Formula:C₂₀H₂₃NO₅
Molecular Weight:357.406
Hs Code.:

methyl 4,5-dimethoxy-2-N-<acetyl(phenylmethyl)amino>benzeneacetate

Synonyms:methyl 4,5-dimethoxy-2-N-benzeneacetate

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Chemical Property of methyl 4,5-dimethoxy-2-N-benzeneacetate

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Technology Process of methyl 4,5-dimethoxy-2-N-benzeneacetate

There total 5 articles about methyl 4,5-dimethoxy-2-N-benzeneacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 118671-08-2
N-Benzyl-N-(2-cyanomethyl-4,5-dimethoxy-phenyl)-acetamide

: 118671-18-4
methyl 4,5-dimethoxy-2-N-benzeneacetate

Guidance literature:: With hydrogenchloride; In methanol; for 2h; Heating;
DOI:10.1016/S0040-4020(01)86867-8

Reference yield:

: 50546-80-0
(2-amino-4,5-dimethoxy-phenyl)-acetonitrile

: 118671-18-4
methyl 4,5-dimethoxy-2-N-benzeneacetate

Guidance literature:: Multi-step reaction with 4 steps

1: p-TosOH / benzene / 16 h / azeotropic removal of water

2: 3M HCl, NaCNBH₃ / methanol / indicated by bromocresol

3: 79 percent / p-TosOH / Heating

4: 79 percent / hydrogen chloride / methanol / 2 h / Heating

With hydrogenchloride; sodium cyanoborohydride; toluene-4-sulfonic acid; In methanol; benzene;
DOI:10.1016/S0040-4020(01)86867-8

Reference yield:

: 100-52-7
benzaldehyde

: 118671-18-4
methyl 4,5-dimethoxy-2-N-benzeneacetate

Guidance literature:: Multi-step reaction with 4 steps

1: p-TosOH / benzene / 16 h / azeotropic removal of water

2: 3M HCl, NaCNBH₃ / methanol / indicated by bromocresol

3: 79 percent / p-TosOH / Heating

4: 79 percent / hydrogen chloride / methanol / 2 h / Heating

With hydrogenchloride; sodium cyanoborohydride; toluene-4-sulfonic acid; In methanol; benzene;
DOI:10.1016/S0040-4020(01)86867-8