4-O-allyl-2,3-di-O-benzoyl-6-deoxy-α-L-talopyranosyl trichloroacetimidate

Base Information

Chemical Name:4-O-allyl-2,3-di-O-benzoyl-6-deoxy-α-L-talopyranosyl trichloroacetimidate
CAS No.:1272616-93-9
Molecular Formula:C₂₅H₂₄Cl₃NO₇
Molecular Weight:556.827
Hs Code.:

Synonyms:4-O-allyl-2,3-di-O-benzoyl-6-deoxy-α-L-talopyranosyl trichloroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-O-allyl-2,3-di-O-benzoyl-6-deoxy-α-L-talopyranosyl trichloroacetimidate

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Technology Process of 4-O-allyl-2,3-di-O-benzoyl-6-deoxy-α-L-talopyranosyl trichloroacetimidate

There total 5 articles about 4-O-allyl-2,3-di-O-benzoyl-6-deoxy-α-L-talopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1272616-91-7
p-methoxyphenyl 4-O-allyl-2,3-di-O-benzoyl-6-deoxy-α-L-talopyranoside

: 1272616-93-9
4-O-allyl-2,3-di-O-benzoyl-6-deoxy-α-L-talopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium cerium (IV) nitrate / acetonitrile / 0.33 h / 35 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 4 h / Inert atmosphere

With ammonium cerium (IV) nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; acetonitrile;
DOI:10.3390/molecules16021113

Reference yield:

: 1096154-15-2
4-methoxyphenyl 6-deoxy-2,3-O-isopropylidene-α-L-talopyranoside

: 1272616-93-9
4-O-allyl-2,3-di-O-benzoyl-6-deoxy-α-L-talopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

2: acetic acid / 2 h / Heating

3: pyridine / 20 °C

4: ammonium cerium (IV) nitrate / acetonitrile / 0.33 h / 35 °C

5: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 4 h / Inert atmosphere

With pyridine; ammonium cerium (IV) nitrate; sodium hydride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.3390/molecules16021113

Reference yield:

: 1272616-88-2
p-methoxyphenyl 4-O-allyl-2,3-O-isopropylidene-6-deoxy-α-L-talopyranoside

: 1272616-93-9
4-O-allyl-2,3-di-O-benzoyl-6-deoxy-α-L-talopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / 2 h / Heating

2: pyridine / 20 °C

3: ammonium cerium (IV) nitrate / acetonitrile / 0.33 h / 35 °C

4: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 4 h / Inert atmosphere

With pyridine; ammonium cerium (IV) nitrate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; acetonitrile;
DOI:10.3390/molecules16021113