(2S,3S)-3-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-(4-nitro-phenoxycarbonylsulfanylmethyl)-4-oxo-azetidine-1-sulfonic acid

Base Information

Chemical Name:(2S,3S)-3-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-(4-nitro-phenoxycarbonylsulfanylmethyl)-4-oxo-azetidine-1-sulfonic acid
CAS No.:176748-50-8
Molecular Formula:C₃₆H₃₀N₆O₁₀S₃
Molecular Weight:802.866
Hs Code.:

(2S,3S)-3-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-(4-nitro-phenoxycarbonylsulfanylmethyl)-4-oxo-azetidine-1-sulfonic acid

Synonyms:(2S,3S)-3-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-(4-nitro-phenoxycarbonylsulfanylmethyl)-4-oxo-azetidine-1-sulfonic acid

Suppliers and Price of (2S,3S)-3-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-(4-nitro-phenoxycarbonylsulfanylmethyl)-4-oxo-azetidine-1-sulfonic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,3S)-3-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-(4-nitro-phenoxycarbonylsulfanylmethyl)-4-oxo-azetidine-1-sulfonic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,3S)-3-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-(4-nitro-phenoxycarbonylsulfanylmethyl)-4-oxo-azetidine-1-sulfonic acid

There total 5 articles about (2S,3S)-3-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-(4-nitro-phenoxycarbonylsulfanylmethyl)-4-oxo-azetidine-1-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 176748-48-4
Thiocarbonic acid S-((2S,3S)-3-{2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-4-oxo-azetidin-2-ylmethyl) ester O-(4-nitro-phenyl) ester

: 176748-50-8
(2S,3S)-3-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-(4-nitro-phenoxycarbonylsulfanylmethyl)-4-oxo-azetidine-1-sulfonic acid

Guidance literature:: With sulfur trioxide; In N,N-dimethyl-formamide; at 0 ℃; for 3h;

Reference yield:

: 176894-32-9
N-((2S,3S)-2-Mercaptomethyl-4-oxo-azetidin-3-yl)-2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetamide

: 176748-50-8
(2S,3S)-3-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-(4-nitro-phenoxycarbonylsulfanylmethyl)-4-oxo-azetidine-1-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / CH₂Cl₂; dimethylformamide / 0.25 h / 0 °C

2: 89 percent / SO₃*DMF / dimethylformamide / 3 h / 0 °C

With sulfur trioxide; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 94105-04-1
N-((2S,3S)-2-Iodomethyl-4-oxo-azetidin-3-yl)-2-[(Z)-methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetamide

: 176748-50-8
(2S,3S)-3-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetylamino}-2-(4-nitro-phenoxycarbonylsulfanylmethyl)-4-oxo-azetidine-1-sulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / NaSH*H₂O / dimethylformamide / 0.25 h / 0 °C

2: 64 percent / CH₂Cl₂; dimethylformamide / 0.25 h / 0 °C

3: 89 percent / SO₃*DMF / dimethylformamide / 3 h / 0 °C

With sodium hydrogensulfide; sulfur trioxide; In dichloromethane; N,N-dimethyl-formamide;