9-(benzylideneamino)-9-borabicyclo{3.3.1}nonane

Base Information

Chemical Name:9-(benzylideneamino)-9-borabicyclo{3.3.1}nonane
CAS No.:143122-91-2
Molecular Formula:C₁₅H₂₀BN
Molecular Weight:225.142
Hs Code.:

Synonyms:9-(benzylideneamino)-9-borabicyclo{3.3.1}nonane

Suppliers and Price of 9-(benzylideneamino)-9-borabicyclo{3.3.1}nonane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(benzylideneamino)-9-borabicyclo{3.3.1}nonane

Chemical Property:

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Technology Process of 9-(benzylideneamino)-9-borabicyclo{3.3.1}nonane

There total 2 articles about 9-(benzylideneamino)-9-borabicyclo{3.3.1}nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 21205-91-4
9-borabicyclo[3.3.1]nonane dimer

: 100-47-0
benzonitrile

: 143122-91-2
9-(benzylideneamino)-9-borabicyclo{3.3.1}nonane

Guidance literature:: In benzonitrile; heating soln. of C16H30B2 in excess of nitrile for 10 h under dry oxygen-free argon;; removal of ecxess nitrile in vac.; distn. at 1E-3 Torr and 105-110°C; solidification on cooling with liquid nitrogen; elem. anal.;;

Reference yield:

: 100-47-0
benzonitrile

: 280-64-8
9-bora-bicyclo[3.3.1]nonane

: 143122-91-2
9-(benzylideneamino)-9-borabicyclo{3.3.1}nonane

Guidance literature:: With C₃₃H₄₇O₂PRuSi₂; In tetrahydrofuran-d8; at 40 ℃; for 0.5h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.organomet.9b00064

Reference yield: 53.0%

: 108-86-1,52753-63-6
bromobenzene

: 143122-91-2
9-(benzylideneamino)-9-borabicyclo{3.3.1}nonane

: 538-51-2
benzylidene phenylamine

Guidance literature:: With potassium tert-butylate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; CyJohnPhos; In tetrahydrofuran; at 60 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.organomet.9b00064