7-(4-hydroxycinnamoyl)-13-acetyl(baccatin III)-14β-hydroxy-1,14-carbonate

Base Information

Chemical Name:7-(4-hydroxycinnamoyl)-13-acetyl(baccatin III)-14β-hydroxy-1,14-carbonate
CAS No.:848250-68-0
Molecular Formula:C₄₃H₄₄O₁₆
Molecular Weight:816.813
Hs Code.:

Synonyms:7-(4-hydroxycinnamoyl)-13-acetyl(baccatin III)-14β-hydroxy-1,14-carbonate

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Chemical Property of 7-(4-hydroxycinnamoyl)-13-acetyl(baccatin III)-14β-hydroxy-1,14-carbonate

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Technology Process of 7-(4-hydroxycinnamoyl)-13-acetyl(baccatin III)-14β-hydroxy-1,14-carbonate

There total 7 articles about 7-(4-hydroxycinnamoyl)-13-acetyl(baccatin III)-14β-hydroxy-1,14-carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: C₄₉H₅₈O₁₆Si

: 848250-68-0
7-(4-hydroxycinnamoyl)-13-acetyl(baccatin III)-14β-hydroxy-1,14-carbonate

Guidance literature:: With pyridine; pyridine hydrogenfluoride; In acetonitrile; at 0 - 25 ℃;
DOI:10.1021/jm049483y

Reference yield:

: 145533-34-2
14-β-hydroxy-10-deacetylbaccatin III

: 848250-68-0
7-(4-hydroxycinnamoyl)-13-acetyl(baccatin III)-14β-hydroxy-1,14-carbonate

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / dimethylformamide / 25 °C

2: pyridine / CH₂Cl₂ / 0 °C

3: 92 percent / DMAP / CH₂Cl₂ / 5 h

4: 98 percent / HF*pyridine; pyridine / acetonitrile / 2 h / 20 °C

5: EDC; DMAP / CH₂Cl₂ / 15 h / 20 °C

6: 92 percent / HF*pyridine; pyridine / acetonitrile / 0 - 25 °C

With pyridine; dmap; pyridine hydrogenfluoride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm049483y

Reference yield:

: 156965-59-2
7-(triethylsilyl)-14β-hydroxy-10-deacetylbaccatin III

: 848250-68-0
7-(4-hydroxycinnamoyl)-13-acetyl(baccatin III)-14β-hydroxy-1,14-carbonate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / CH₂Cl₂ / 0 °C

2: 92 percent / DMAP / CH₂Cl₂ / 5 h

3: 98 percent / HF*pyridine; pyridine / acetonitrile / 2 h / 20 °C

4: EDC; DMAP / CH₂Cl₂ / 15 h / 20 °C

5: 92 percent / HF*pyridine; pyridine / acetonitrile / 0 - 25 °C

With pyridine; dmap; pyridine hydrogenfluoride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; acetonitrile;
DOI:10.1021/jm049483y