Technology Process of C16H21NO3S
There total 24 articles about C16H21NO3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium diisopropyl amide;
In
tetrahydrofuran; hexane;
at -78 - 0 ℃;
for 0.583333h;
DOI:10.1021/jo400324t
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium chloride / 3.5 h / -20 - 20 °C
2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C
2.2: 2 h
3.1: methanol; lithium borohydride / tetrahydrofuran / 2.67 h / 0 - 20 °C
4.1: tributylphosphine / tetrahydrofuran / 12.5 h / 0 - 20 °C
5.1: dihydrogen peroxide; hexaammonium heptamolybdate tetrahydrate / water; ethanol / 12 h
6.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.58 h / -78 - 0 °C
With
methanol; lithium borohydride; hexaammonium heptamolybdate tetrahydrate; tributylphosphine; dihydrogen peroxide; sodium hexamethyldisilazane; lithium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; ethanol; hexane; water;
DOI:10.1021/jo400324t
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: toluene-4-sulfonic acid / acetone / 0.33 h
2.1: 2-methyl-but-2-ene; sodium dihydrogen phosphate monohydrate; Na(1+)*Cl2O / water; tert-butyl alcohol / 2.5 h
3.1: triethylamine; pivaloyl chloride / tetrahydrofuran / 3 h / -20 °C
4.1: lithium chloride / 3.5 h / -20 - 20 °C
5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C
5.2: 1 h
6.1: methanol; lithium borohydride / tetrahydrofuran / 2.67 h / 0 - 20 °C
7.1: dihydrogen peroxide; hexaammonium heptamolybdate tetrahydrate / water; ethanol / 12 h
8.1: triphenylphosphine; 1H-imidazole; iodine / tetrahydrofuran / 3.42 h / 0 - 20 °C
9.1: hydrogen; palladium on carbon / ethanol / 18 h / 760.05 Torr / Inert atmosphere
10.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.58 h / -78 - 0 °C
With
1H-imidazole; methanol; lithium borohydride; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; hexaammonium heptamolybdate tetrahydrate; palladium on carbon; Na(1+)*Cl2O; hydrogen; dihydrogen peroxide; iodine; sodium hexamethyldisilazane; pivaloyl chloride; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; lithium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; ethanol; hexane; water; acetone; tert-butyl alcohol;
DOI:10.1021/jo400324t
