(2R,3R)-cis-1-(N-1-bis(4-methoxyphenyl)methyl)-2-carboxyethyl-3-cyclohexylaziridine

Base Information

Chemical Name:(2R,3R)-cis-1-(N-1-bis(4-methoxyphenyl)methyl)-2-carboxyethyl-3-cyclohexylaziridine
CAS No.:943348-73-0
Molecular Formula:C₂₆H₃₃NO₄
Molecular Weight:423.552
Hs Code.:

Synonyms:(2R,3R)-cis-1-(N-1-bis(4-methoxyphenyl)methyl)-2-carboxyethyl-3-cyclohexylaziridine

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Chemical Property of (2R,3R)-cis-1-(N-1-bis(4-methoxyphenyl)methyl)-2-carboxyethyl-3-cyclohexylaziridine

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Technology Process of (2R,3R)-cis-1-(N-1-bis(4-methoxyphenyl)methyl)-2-carboxyethyl-3-cyclohexylaziridine

There total 7 articles about (2R,3R)-cis-1-(N-1-bis(4-methoxyphenyl)methyl)-2-carboxyethyl-3-cyclohexylaziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 623-73-4
diazoacetic acid ethyl ester

: N-cyclohexylmethylidene-bis(4-methoxyphenyl)methylamine

: 943348-73-0
(2R,3R)-cis-1-(N-1-bis(4-methoxyphenyl)methyl)-2-carboxyethyl-3-cyclohexylaziridine

: C₂₆H₃₃NO₄

: C₂₆H₃₃NO₄

: (2S,3S)-cis-1-(N-1-bis(4-methoxyphenyl)methyl)-2-carboxyethyl-3-cyclohexylaziridine

Guidance literature:: (3S)-(+)-2,2'-diphenyl-(3,3'-biphenanthrene)-4,4'-diol; In tetrachloromethane; at 25 ℃; for 24h;
DOI:10.1021/ja069371r

Reference yield: 3.0%

: 623-73-4
diazoacetic acid ethyl ester

: N-cyclohexylmethylidene-bis(4-methoxyphenyl)methylamine

: 943348-73-0
(2R,3R)-cis-1-(N-1-bis(4-methoxyphenyl)methyl)-2-carboxyethyl-3-cyclohexylaziridine

: trans-1-(N-1-bis(4-methoxyphenyl)methyl)-2-carboxyethyl-3-cyclohexylaziridine

: C₂₆H₃₃NO₄

: (2S,3S)-cis-1-(N-1-bis(4-methoxyphenyl)methyl)-2-carboxyethyl-3-cyclohexylaziridine

Guidance literature:: (3S)-(+)-2,2'-diphenyl-(3,3'-biphenanthrene)-4,4'-diol; In dichloromethane; at 25 ℃; for 24h; Further byproducts.;
DOI:10.1021/ja069371r

Reference yield:

: 19293-62-0
p,p'-dimethoxybenzhydrylamine

: 943348-73-0
(2R,3R)-cis-1-(N-1-bis(4-methoxyphenyl)methyl)-2-carboxyethyl-3-cyclohexylaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / MgSO₄ / CH₂Cl₂ / 24 h / 25 °C

2: (S)-VAPOL; triphenyl borate / CH₂Cl₂ / 24 h / 25 °C

With magnesium sulfate; (3S)-(+)-2,2'-diphenyl-(3,3'-biphenanthrene)-4,4'-diol; In dichloromethane;
DOI:10.1021/ja069371r