C₃₇H₃₂N₂O₂S

Base Information

Chemical Name:C₃₇H₃₂N₂O₂S
CAS No.:1414888-83-7
Molecular Formula:C₃₇H₃₂N₂O₂S
Molecular Weight:568.739
Hs Code.:

C<sub>37</sub>H<sub>32</sub>N<sub>2</sub>O<sub>2</sub>S

Synonyms:C₃₇H₃₂N₂O₂S

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Chemical Property of C₃₇H₃₂N₂O₂S

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Technology Process of C₃₇H₃₂N₂O₂S

There total 7 articles about C₃₇H₃₂N₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1414888-92-8
C₃₇H₃₃N₂O₂⁽¹⁺⁾*Cl^(1-)

: 1414888-83-7
C₃₇H₃₂N₂O₂S

Guidance literature:: C₃₇H₃₃N₂O₂⁽¹⁺⁾*Cl^(1-); With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere;

With sulfur; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.09.116 DOI:10.1016/j.tetlet.2012.09.116

Reference yield:

: 626-15-3
1,3-bis-(bromomethyl)benzene

: 1414888-83-7
C₃₇H₃₂N₂O₂S

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / acetonitrile / Reflux; Inert atmosphere

2.1: sodium tetrahydroborate / methanol / 20 °C / Inert atmosphere

3.1: phosphorus tribromide / dichloromethane / 20 °C / Inert atmosphere

4.1: potassium carbonate; tetraethylammonium bromide / acetonitrile / 48 h / Reflux; Inert atmosphere

5.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 2 h / Inert atmosphere

5.2: 24 h / 125 °C / Inert atmosphere

6.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

6.2: 2 h / 20 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; potassium tert-butylate; tetraethylammonium bromide; phosphorus tribromide; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2012.09.116 DOI:10.1016/j.tetlet.2012.09.116

Reference yield:

: 565462-34-2
{4-[3-(4-hydroxymethyl-phenoxymethyl)-benzyloxy]-phenyl}-methanol

: 1414888-83-7
C₃₇H₃₂N₂O₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: phosphorus tribromide / dichloromethane / 20 °C / Inert atmosphere

2.1: potassium carbonate; tetraethylammonium bromide / acetonitrile / 48 h / Reflux; Inert atmosphere

3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 2 h / Inert atmosphere

3.2: 24 h / 125 °C / Inert atmosphere

4.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

4.2: 2 h / 20 °C / Inert atmosphere

With hydrogenchloride; potassium tert-butylate; tetraethylammonium bromide; phosphorus tribromide; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2012.09.116 DOI:10.1016/j.tetlet.2012.09.116