bis(2,2,2-trichloroethyl) exo,exo-2,5-diphenyl-7-oxa-3,4-diazabicyclo<4.1.0>heptane-3,4-dicarboxylate

Base Information

• Chemical Name: bis(2,2,2-trichloroethyl) exo,exo-2,5-diphenyl-7-oxa-3,4-diazabicyclo<4.1.0>heptane-3,4-dicarboxylate
• CAS No.: 98760-58-8
• Molecular Formula: C₂₂H₁₈Cl₆N₂O₅
• Molecular Weight: 603.113

Synonyms:bis(2,2,2-trichloroethyl) exo,exo-2,5-diphenyl-7-oxa-3,4-diazabicyclo<4.1.0>heptane-3,4-dicarboxylate

Chemical Property of bis(2,2,2-trichloroethyl) exo,exo-2,5-diphenyl-7-oxa-3,4-diazabicyclo<4.1.0>heptane-3,4-dicarboxylate

Chemical Property:

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Technology Process of bis(2,2,2-trichloroethyl) exo,exo-2,5-diphenyl-7-oxa-3,4-diazabicyclo<4.1.0>heptane-3,4-dicarboxylate

There total 3 articles about bis(2,2,2-trichloroethyl) exo,exo-2,5-diphenyl-7-oxa-3,4-diazabicyclo<4.1.0>heptane-3,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

bis(2,2,2-trichloroethyl) 3,6-diphenyl-1,2,3,6-tetrahydropyridazine-1,2-dicarboxylate (98760-57-7) → bis(2,2,2-trichloroethyl) exo,exo-2,5-diphenyl-7-oxa-3,4-diazabicyclo<4.1.0>heptane-3,4-dicarboxylate (98760-58-8)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In chloroform; at 0 - 20 ℃; for 72h;

DOI:10.1021/jo00224a050

Reference yield:

trans,trans-1,4-Diphenyl-1,3-butadiene (886-65-7,538-81-8) → bis(2,2,2-trichloroethyl) exo,exo-2,5-diphenyl-7-oxa-3,4-diazabicyclo<4.1.0>heptane-3,4-dicarboxylate (98760-58-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / toluene / 3 h / 85 °C

2: 57 percent / sodium bicarbonate, m-chloroperbenzoic acid / CHCl₃ / 72 h / 0 - 20 °C

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In chloroform; toluene;

DOI:10.1021/jo00224a050

Reference yield:

bis(2,2,2-trichlorethyl)azodicarboxylate (38857-88-4) → bis(2,2,2-trichloroethyl) exo,exo-2,5-diphenyl-7-oxa-3,4-diazabicyclo<4.1.0>heptane-3,4-dicarboxylate (98760-58-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / toluene / 3 h / 85 °C

2: 57 percent / sodium bicarbonate, m-chloroperbenzoic acid / CHCl₃ / 72 h / 0 - 20 °C

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In chloroform; toluene;

DOI:10.1021/jo00224a050

upstream raw materials:

bis(2,2,2-trichloroethyl) 3,6-diphenyl-1,2,3,6-tetrahydropyridazine-1,2-dicarboxylate

trans,trans-1,4-Diphenyl-1,3-butadiene

bis(2,2,2-trichlorethyl)azodicarboxylate

Downstream raw materials:

trans,trans-bis(2-phenylvinyl) ether

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