3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid 2-(trimethylsilyl)ethyl ester

Base Information

Chemical Name:3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid 2-(trimethylsilyl)ethyl ester
CAS No.:319909-84-7
Molecular Formula:C₂₇H₃₉N₃O₅Si
Molecular Weight:513.709
Hs Code.:

Synonyms:3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid 2-(trimethylsilyl)ethyl ester

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Chemical Property of 3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid 2-(trimethylsilyl)ethyl ester

Chemical Property:

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Technology Process of 3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid 2-(trimethylsilyl)ethyl ester

There total 1 articles about 3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid 2-(trimethylsilyl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7693-46-1
4-Nitrophenyl chloroformate

: 103-67-3
benzyl-methyl-amine

: 206441-79-4
6-amino-3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methylbenzoic 2-(trimethylsilyl)ethyl ester

: 319909-84-7
3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid 2-(trimethylsilyl)ethyl ester

Guidance literature:: 4-Nitrophenyl chloroformate; 6-amino-3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methylbenzoic 2-(trimethylsilyl)ethyl ester; In dichloromethane; at 20 ℃; for 3h;

benzyl-methyl-amine; In dichloromethane; at 20 ℃; for 15h;

With 4,5,6,7-tetrafluoroisobenzofuran-1,3-dione; Amberlyst A-21; more than 3 stages;

Reference yield:

: 319909-84-7
3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid 2-(trimethylsilyl)ethyl ester

: 319909-85-8
3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid

Guidance literature:: 3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid 2-(trimethylsilyl)ethyl ester; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;

In tetrahydrofuran;

Reference yield:

: 319909-84-7
3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid 2-(trimethylsilyl)ethyl ester

: 319909-86-9
3-amino-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid 2-(trimethylsilyl)ethyl ester

Guidance literature:: 3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-methyl-6-[[[methyl(phenylmethyl)-amino]carbonyl]amino]benzoic acid 2-(trimethylsilyl)ethyl ester; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

With Amberlyst A-21; In DMF (N,N-dimethyl-formamide); dichloromethane; for 1h;