cyclohex-2-en-1-yl 4-acetoxybenzoate

Base Information

• Chemical Name: cyclohex-2-en-1-yl 4-acetoxybenzoate
• CAS No.: 1383677-48-2
• Molecular Formula: C₁₅H₁₆O₄
• Molecular Weight: 260.29
• Mol file: 1383677-48-2.mol

Synonyms:cyclohex-2-en-1-yl 4-acetoxybenzoate

Chemical Property of cyclohex-2-en-1-yl 4-acetoxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of cyclohex-2-en-1-yl 4-acetoxybenzoate

There total 2 articles about cyclohex-2-en-1-yl 4-acetoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4-acetyloxy-benzoic acid (2345-34-8) + cyclohexane (110-82-7,25012-93-5) → cyclohex-2-en-1-yl 4-acetoxybenzoate (1383677-48-2)

Guidance literature:

With tert.-butylhydroperoxide; (6,8,15,17-tetramethyldibenzo[b,i][1,4,8,11]tetraazacyclotetradecinato)copper(II); In neat (no solvent); at 80 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1016/j.ica.2019.119190

Reference yield: 49.0%

4-acetyloxy-benzoic acid (2345-34-8) + cyclohexene (110-83-8) → cyclohex-2-en-1-yl 4-acetoxybenzoate (1383677-48-2)

Guidance literature:

With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; In benzene; at 80 ℃; for 8h;

DOI:10.1021/ol3013606

upstream raw materials:

4-acetyloxy-benzoic acid

cyclohexene

cyclohexane