2-methoxy-4-((E)-3-(4-morpholinobutoxy)-3-oxoprop-1-enyl)-phenyl-2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

Base Information

Chemical Name:2-methoxy-4-((E)-3-(4-morpholinobutoxy)-3-oxoprop-1-enyl)-phenyl-2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate
CAS No.:1613704-75-8
Molecular Formula:C₄₀H₅₃NO₆S
Molecular Weight:675.93
Hs Code.:

Synonyms:2-methoxy-4-((E)-3-(4-morpholinobutoxy)-3-oxoprop-1-enyl)-phenyl-2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

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Chemical Property of 2-methoxy-4-((E)-3-(4-morpholinobutoxy)-3-oxoprop-1-enyl)-phenyl-2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

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Technology Process of 2-methoxy-4-((E)-3-(4-morpholinobutoxy)-3-oxoprop-1-enyl)-phenyl-2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

There total 3 articles about 2-methoxy-4-((E)-3-(4-morpholinobutoxy)-3-oxoprop-1-enyl)-phenyl-2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1613704-61-2
C₁₈H₂₅NO₅

: 162520-00-5
salirasib

: 1613704-75-8
2-methoxy-4-((E)-3-(4-morpholinobutoxy)-3-oxoprop-1-enyl)-phenyl-2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1039/c4ob00023d

Reference yield:

: 1135-24-6,537-98-4
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid

: 1613704-75-8
2-methoxy-4-((E)-3-(4-morpholinobutoxy)-3-oxoprop-1-enyl)-phenyl-2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / acetone / 4 h / 50 °C

2: potassium iodide; potassium carbonate / acetonitrile / 50 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 16 h / 20 °C

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium iodide; In dichloromethane; acetone; acetonitrile;
DOI:10.1039/c4ob00023d

Reference yield:

: 410071-23-7
(E)-4-bromobutyl 3-(4-hydroxy-3-methoxyphenyl)acrylate

: 1613704-75-8
2-methoxy-4-((E)-3-(4-morpholinobutoxy)-3-oxoprop-1-enyl)-phenyl-2-((2E,6E)-3,7,11-trimethyldodeca-2,6,10-trienylthio)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium iodide; potassium carbonate / acetonitrile / 50 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 16 h / 20 °C

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium iodide; In dichloromethane; acetonitrile;
DOI:10.1039/c4ob00023d