dimethyl 2-(5-methyl-2-((3-phenylprop-2-yn-1-yl)oxy)phenyl)cyclopropane-1,1-dicarboxylate

Base Information

Chemical Name:dimethyl 2-(5-methyl-2-((3-phenylprop-2-yn-1-yl)oxy)phenyl)cyclopropane-1,1-dicarboxylate
CAS No.:1383545-72-9
Molecular Formula:C₂₃H₂₂O₅
Molecular Weight:378.425
Hs Code.:

Synonyms:dimethyl 2-(5-methyl-2-((3-phenylprop-2-yn-1-yl)oxy)phenyl)cyclopropane-1,1-dicarboxylate

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Chemical Property of dimethyl 2-(5-methyl-2-((3-phenylprop-2-yn-1-yl)oxy)phenyl)cyclopropane-1,1-dicarboxylate

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Technology Process of dimethyl 2-(5-methyl-2-((3-phenylprop-2-yn-1-yl)oxy)phenyl)cyclopropane-1,1-dicarboxylate

There total 4 articles about dimethyl 2-(5-methyl-2-((3-phenylprop-2-yn-1-yl)oxy)phenyl)cyclopropane-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₀O₅

: 1774-47-6
trimethylsulfoxonium iodide

: 1383545-72-9
dimethyl 2-(5-methyl-2-((3-phenylprop-2-yn-1-yl)oxy)phenyl)cyclopropane-1,1-dicarboxylate

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 0 - 50 ℃; for 3h; Inert atmosphere;
DOI:10.1002/asia.201200104

Reference yield:

: 1087606-32-3
5-methyl-2-(prop-2-ynyloxy)benzaldehyde

: 1383545-72-9
dimethyl 2-(5-methyl-2-((3-phenylprop-2-yn-1-yl)oxy)phenyl)cyclopropane-1,1-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / Inert atmosphere

2: piperidine / chloroform / Reflux

3: sodium hydride / dimethyl sulfoxide / 3 h / 0 - 50 °C / Inert atmosphere

With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium hydride; triethylamine; In tetrahydrofuran; chloroform; dimethyl sulfoxide;
DOI:10.1002/asia.201200104

Reference yield:

: C₁₇H₁₄O₂

: 1383545-72-9
dimethyl 2-(5-methyl-2-((3-phenylprop-2-yn-1-yl)oxy)phenyl)cyclopropane-1,1-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / chloroform / Reflux

2: sodium hydride / dimethyl sulfoxide / 3 h / 0 - 50 °C / Inert atmosphere

With piperidine; sodium hydride; In chloroform; dimethyl sulfoxide;
DOI:10.1002/asia.201200104