N-(benzoyloxy)-N-[1-((6-chloropyridin-3-yl)methyl)pyridin-2(1H)-ylidene]-2,2,2-trifluoroacetimidamide

Base Information

Chemical Name:N-(benzoyloxy)-N-[1-((6-chloropyridin-3-yl)methyl)pyridin-2(1H)-ylidene]-2,2,2-trifluoroacetimidamide
CAS No.:1453496-35-9
Molecular Formula:C₂₀H₁₄ClF₃N₄O₂
Molecular Weight:434.805
Hs Code.:

Synonyms:N-(benzoyloxy)-N-[1-((6-chloropyridin-3-yl)methyl)pyridin-2(1H)-ylidene]-2,2,2-trifluoroacetimidamide

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Chemical Property of N-(benzoyloxy)-N-[1-((6-chloropyridin-3-yl)methyl)pyridin-2(1H)-ylidene]-2,2,2-trifluoroacetimidamide

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Technology Process of N-(benzoyloxy)-N-[1-((6-chloropyridin-3-yl)methyl)pyridin-2(1H)-ylidene]-2,2,2-trifluoroacetimidamide

There total 7 articles about N-(benzoyloxy)-N-[1-((6-chloropyridin-3-yl)methyl)pyridin-2(1H)-ylidene]-2,2,2-trifluoroacetimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1453496-34-8
N-[1-((6-chloropyridin-3-yl)methyl)pyridin-2(1H)-ylidene]-2,2,2-trifluoro-N'-hydroxyacetimidamide

: 98-88-4
benzoyl chloride

: 1453496-35-9
N-(benzoyloxy)-N-[1-((6-chloropyridin-3-yl)methyl)pyridin-2(1H)-ylidene]-2,2,2-trifluoroacetimidamide

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 0.166667h;

Reference yield:

: 1363400-41-2
N-[1-[(6-chloro-3-pyridinyl)methyl]-2(1H)-pyridinylidene]-2,2,2-trifluoro-acetamide

: 1453496-35-9
N-(benzoyloxy)-N-[1-((6-chloropyridin-3-yl)methyl)pyridin-2(1H)-ylidene]-2,2,2-trifluoroacetimidamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetraphosphorus decasulfide; sodium carbonate / toluene; ethyl acetate / 19.17 h / 50 °C

2: hydroxylamine hydrochloride; triethylamine / ethyl acetate; ethanol / 21.5 h / 50 °C

3: triethylamine / acetonitrile / 0.17 h / 20 °C

With tetraphosphorus decasulfide; hydroxylamine hydrochloride; sodium carbonate; triethylamine; In ethanol; ethyl acetate; toluene; acetonitrile;

Reference yield:

: 504-29-0
2-aminopyridine

: 1453496-35-9
N-(benzoyloxy)-N-[1-((6-chloropyridin-3-yl)methyl)pyridin-2(1H)-ylidene]-2,2,2-trifluoroacetimidamide

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 2.25 h / 0 - 20 °C

2: potassium carbonate / acetonitrile / 16 h / 20 °C / Reflux

3: tetraphosphorus decasulfide; sodium carbonate / toluene; ethyl acetate / 19.17 h / 50 °C

4: hydroxylamine hydrochloride; triethylamine / ethyl acetate; ethanol / 21.5 h / 50 °C

5: triethylamine / acetonitrile / 0.17 h / 20 °C

With tetraphosphorus decasulfide; hydroxylamine hydrochloride; sodium carbonate; potassium carbonate; triethylamine; In ethanol; dichloromethane; ethyl acetate; toluene; acetonitrile;