3-(β-D-glucopyranosyl)-2-[(4-bromobenzylidene)hydrazono]-4-phenyl-2,3-dihydrothiazole

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Chemical Name:3-(β-D-glucopyranosyl)-2-[(4-bromobenzylidene)hydrazono]-4-phenyl-2,3-dihydrothiazole
CAS No.:1416961-43-7
Molecular Formula:C₂₂H₂₂BrN₃O₅S
Molecular Weight:520.404
Hs Code.:

Synonyms:3-(β-D-glucopyranosyl)-2-[(4-bromobenzylidene)hydrazono]-4-phenyl-2,3-dihydrothiazole

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Chemical Property of 3-(β-D-glucopyranosyl)-2-[(4-bromobenzylidene)hydrazono]-4-phenyl-2,3-dihydrothiazole

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Technology Process of 3-(β-D-glucopyranosyl)-2-[(4-bromobenzylidene)hydrazono]-4-phenyl-2,3-dihydrothiazole

There total 3 articles about 3-(β-D-glucopyranosyl)-2-[(4-bromobenzylidene)hydrazono]-4-phenyl-2,3-dihydrothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1416961-42-6
3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2-[(4-bromobenzylidene)hydrazono]-4-phenyl-2,3-dihydrothiazole

: 1416961-43-7
3-(β-D-glucopyranosyl)-2-[(4-bromobenzylidene)hydrazono]-4-phenyl-2,3-dihydrothiazole

Guidance literature:: With ammonia; In methanol; at 20 ℃; for 4h;
DOI:10.1002/jhet.900

Reference yield:

: 307325-15-1
2-[(4-bromobenzylidene)hydrazono]-4-phenyl-2,3-dihydrothiazole

: 1416961-43-7
3-(β-D-glucopyranosyl)-2-[(4-bromobenzylidene)hydrazono]-4-phenyl-2,3-dihydrothiazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / acetone; water / 20 °C

2: ammonia / methanol / 4 h / 20 °C

With ammonia; potassium hydroxide; In methanol; water; acetone;
DOI:10.1002/jhet.900

Reference yield:

: 36449-43-1
2-(4-bromobenzylidene)hydrazine carbothioamide

: 1416961-43-7
3-(β-D-glucopyranosyl)-2-[(4-bromobenzylidene)hydrazono]-4-phenyl-2,3-dihydrothiazole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate / ethanol / 3 h / Reflux

2: potassium hydroxide / acetone; water / 20 °C

3: ammonia / methanol / 4 h / 20 °C

With ammonia; sodium acetate; potassium hydroxide; In methanol; ethanol; water; acetone;
DOI:10.1002/jhet.900