C₆₅H₁₁₂O₁₅Si₃

Base Information

Chemical Name:C₆₅H₁₁₂O₁₅Si₃
CAS No.:410077-81-5
Molecular Formula:C₆₅H₁₁₂O₁₅Si₃
Molecular Weight:1217.85
Hs Code.:

C<sub>65</sub>H<sub>112</sub>O<sub>15</sub>Si<sub>3</sub>

Synonyms:C₆₅H₁₁₂O₁₅Si₃

Suppliers and Price of C₆₅H₁₁₂O₁₅Si₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₅H₁₁₂O₁₅Si₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₅H₁₁₂O₁₅Si₃

There total 35 articles about C₆₅H₁₁₂O₁₅Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: C₆₃H₁₁₀O₁₄Si₃

: 75-36-5
acetyl chloride

: 410077-81-5
C₆₅H₁₁₂O₁₅Si₃

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/ol017273z

Reference yield: 88.0%

: 75-36-5
acetyl chloride

: C₆₃H₁₁₀O₁₄Si₃

: 410077-81-5
C₆₅H₁₁₂O₁₅Si₃

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2009.04.003

Reference yield:

: 410077-68-8
(S)-4-(Naphthalen-2-ylmethoxy)-1-(S)-oxiranyl-butan-2-ol

: 410077-81-5
C₆₅H₁₁₂O₁₅Si₃

Guidance literature:: Multi-step reaction with 13 steps

1.1: 90 percent / imidazole / tetrahydrofuran / 1 h

2.1: t-BuLi / diethyl ether; pentane / 0.83 h / -78 - -45 °C

2.2: diethyl ether; pentane / 4 h / -45 - -20 °C

2.3: 58 percent / HMPA; n-BuLi / hexane; diethyl ether; tetrahydrofuran / 15 h / -20 °C

3.1: Hg(ClO₄)2*4H₂O / acetonitrile; H₂O; CH₂Cl₂ / 0.17 h / 0 °C

3.2: 83 percent / HClO₄ / acetonitrile; H₂O; CH₂Cl₂ / 0.08 h

4.1: 90 percent / pyridine; 4-DMAP / CH₂Cl₂ / 13 h

5.1: 100 percent / 2,6-lutidine / CH₂Cl₂ / -78 - 0 °C

6.1: 98 percent / 2-methylcyclohexadiene; calcium carbonate / Pd(OH)2/C / ethanol / 5.5 h / 70 °C

7.1: 99 percent / Dess-Martin periodinane; pyridine / CH₂Cl₂ / 0.33 h

8.1: 100 percent / NaClO₂; NaH₂PO₄; 2-methyl-2-butene / ethyl-1-propenyl ether / H₂O; tetrahydrofuran; 2-methyl-propan-2-ol / 6 h / 20 °C

9.1: 97 percent / Et₃N / CH₂Cl₂; tetrahydrofuran / 0.5 h

10.1: 91 percent / DDQ / CH₂Cl₂; H₂O / 2 h / 0 °C

11.1: 89 percent / Dess-Martin periodinane; pyridine / CH₂Cl₂ / 1 h

12.1: dicyclohexylboron chloride; triethylamine / pentane / -78 - 0 °C

12.2: pentane / 6.5 h / -78 °C

12.3: 64 percent / H₂O₂ / pentane; methanol / 1 h / 0 °C / pH 7

13.1: 88 percent / pyridine / CH₂Cl₂ / 24 h / 20 °C

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; mercury(II) perchlorate; 2-methyl-but-2-ene; 2-methylcyclohexa-1,3-diene; dicyclohexylboron chloride; tert.-butyl lithium; Dess-Martin periodane; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; calcium carbonate; palladium dihydroxide; ethyl-1-propenyl ether; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; acetonitrile; tert-butyl alcohol; pentane; 7.1: Dess-Martin oxidation / 11.1: Dess-Martin oxidation;
DOI:10.1021/ol017273z