C₁₅H₁₉NO₃S

Base Information

• Chemical Name: C₁₅H₁₉NO₃S
• CAS No.: 1372714-31-2
• Molecular Formula: C₁₅H₁₉NO₃S
• Molecular Weight: 293.387
• Mol file: 1372714-31-2.mol

Synonyms:C₁₅H₁₉NO₃S

Chemical Property of C₁₅H₁₉NO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₉NO₃S

There total 3 articles about C₁₅H₁₉NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(Z)-N-(but-2-yn-1-yl)-N-(4-hydroxybut-2-en-1-yl)-4-methylbenzenesulfonamide (1309600-02-9) → C15H19NO3S (1372714-31-2)

Guidance literature:

With platinum(IV) chloride; In 1,4-dioxane; at 90 ℃; for 16h; stereoselective reaction; Inert atmosphere;

DOI:10.1055/s-0031-1290314

Reference yield:

4-methyl-N-(prop-1-yn-1-yl)benzenesulfonamide (286376-23-6) → C15H19NO3S (1372714-31-2)

Guidance literature:

Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere

3: platinum(IV) chloride / 1,4-dioxane / 16 h / 90 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; platinum(IV) chloride; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane;

DOI:10.1055/s-0031-1290314

Reference yield:

C21H33NO3SSi (1372714-62-9) → C15H19NO3S (1372714-31-2)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere

2: platinum(IV) chloride / 1,4-dioxane / 16 h / 90 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; platinum(IV) chloride; In tetrahydrofuran; 1,4-dioxane;

DOI:10.1055/s-0031-1290314

upstream raw materials:

(Z)-N-(but-2-yn-1-yl)-N-(4-hydroxybut-2-en-1-yl)-4-methylbenzenesulfonamide

C₂₁H₃₃NO₃SSi

4-methyl-N-(prop-1-yn-1-yl)benzenesulfonamide