(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid dimethyl ester

Base Information

Chemical Name:(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid dimethyl ester
CAS No.:73872-72-7
Molecular Formula:C₂₆H₃₂N₂O₈
Molecular Weight:500.549
Hs Code.:

Synonyms:(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid dimethyl ester

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Chemical Property of (S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid dimethyl ester

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Technology Process of (S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid dimethyl ester

There total 6 articles about (S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 218443-11-9
(S,S)-diaminooctanedioic acid dimethyl ester

: 73872-72-7
(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid dimethyl ester

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; water; at 0 - 20 ℃; for 8h;
DOI:10.1002/(SICI)1522-2675(19981111)81:11<2053::AID-HLCA2053>3.0.CO;2-4

Reference yield: 85.0%

: 210985-57-2
(2Z,6Z)-2,7-bis(benzyloxycarbonylamino)-octa-2,6-diene-1,8-dioic acid dimethyl ester

: 73872-72-7
(S,S)-2,7-bis<<(benzyloxy)carbonyl>amino>octanedioic acid dimethyl ester

: (2S,7R)-2,7-Bis-benzyloxycarbonylamino-octanedioic acid dimethyl ester

Guidance literature:: With (+)-1,2-bis-((2S,5S)-2,5-diethylphospholano)benzene(cyclooctadiene)rhodium(I) trifluoromethanesulfonate; hydrogen; In methanol; for 18h; under 3000.24 Torr; Yields of byproduct given; Ambient temperature;
DOI:10.1021/jo982034j