(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)-phenoxy]-1-(3,4,5-trimethoxyphenyl)propyl acetate

Base Information

Chemical Name:(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)-phenoxy]-1-(3,4,5-trimethoxyphenyl)propyl acetate
CAS No.:916264-20-5
Molecular Formula:C₂₅H₃₂O₈
Molecular Weight:460.524
Hs Code.:

Synonyms:(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)-phenoxy]-1-(3,4,5-trimethoxyphenyl)propyl acetate

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Chemical Property of (1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)-phenoxy]-1-(3,4,5-trimethoxyphenyl)propyl acetate

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Technology Process of (1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)-phenoxy]-1-(3,4,5-trimethoxyphenyl)propyl acetate

There total 4 articles about (1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)-phenoxy]-1-(3,4,5-trimethoxyphenyl)propyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 916264-32-9
Acetic acid (1R,2S)-2-hydroxy-1-(3,4,5-trimethoxy-phenyl)-propyl ester

: 916264-20-5
(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)-phenoxy]-1-(3,4,5-trimethoxyphenyl)propyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / triethylamine / toluene / 0 - 20 °C

2: 70 percent / Cs₂CO₃; 18-crown-6 ether / dimethylformamide / 0.17 h / 120 °C / 1500.12 Torr / microwave irradiation

With 18-crown-6 ether; caesium carbonate; triethylamine; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo061521t

Reference yield:

: 916264-16-9
(1R,2S)-2-(4-methoxybenzyloxy)-1-(3,4,5-trimethoxyphenyl)propan-1-ol

: 916264-20-5
(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)-phenoxy]-1-(3,4,5-trimethoxyphenyl)propyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / triethylamine; 4-(dimethylamino)pyridine / acetonitrile / 1 h / 20 °C

2: 80 percent / DDQ / CH₂Cl₂; H₂O / 3 h / 20 °C

3: 100 percent / triethylamine / toluene / 0 - 20 °C

4: 70 percent / Cs₂CO₃; 18-crown-6 ether / dimethylformamide / 0.17 h / 120 °C / 1500.12 Torr / microwave irradiation

With dmap; 18-crown-6 ether; caesium carbonate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/jo061521t

Reference yield:

: 916264-31-8
Acetic acid (1R,2S)-2-(4-methoxy-benzyloxy)-1-(3,4,5-trimethoxy-phenyl)-propyl ester

: 916264-20-5
(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)-phenoxy]-1-(3,4,5-trimethoxyphenyl)propyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / DDQ / CH₂Cl₂; H₂O / 3 h / 20 °C

2: 100 percent / triethylamine / toluene / 0 - 20 °C

3: 70 percent / Cs₂CO₃; 18-crown-6 ether / dimethylformamide / 0.17 h / 120 °C / 1500.12 Torr / microwave irradiation

With 18-crown-6 ether; caesium carbonate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo061521t