(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)phenoxy]-1-(3,4,5-trimethoxyphenyl)propan-1-ol

Base Information

Chemical Name:(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)phenoxy]-1-(3,4,5-trimethoxyphenyl)propan-1-ol
CAS No.:658706-47-9
Molecular Formula:C₂₃H₃₀O₇
Molecular Weight:418.487
Hs Code.:

Synonyms:(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)phenoxy]-1-(3,4,5-trimethoxyphenyl)propan-1-ol

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Chemical Property of (1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)phenoxy]-1-(3,4,5-trimethoxyphenyl)propan-1-ol

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Technology Process of (1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)phenoxy]-1-(3,4,5-trimethoxyphenyl)propan-1-ol

There total 20 articles about (1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)phenoxy]-1-(3,4,5-trimethoxyphenyl)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 916264-20-5
(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)-phenoxy]-1-(3,4,5-trimethoxyphenyl)propyl acetate

: 658706-47-9
(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)phenoxy]-1-(3,4,5-trimethoxyphenyl)propan-1-ol

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 1h;
DOI:10.1021/jo061521t

Reference yield: 97.0%

: (1R,2R)-2-[4-allyl-(2,6-dimethoxyphenoxy)-1-(3,4,5-trimethoxyphenyl)]propan-1-ol

: 658706-47-9
(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)phenoxy]-1-(3,4,5-trimethoxyphenyl)propan-1-ol

Guidance literature:: With palladium dichloride; In methanol; at 20 ℃; Inert atmosphere;
DOI:10.1055/s-0031-1290678

Reference yield:

: 6627-88-9
4-allyl-2,6-dimethoxyphenol

: 658706-47-9
(1R,2R)-2-[2,6-dimethoxy-4-((E)-prop-1-enyl)phenoxy]-1-(3,4,5-trimethoxyphenyl)propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / PdCl₂ / methanol / 24 h / 20 °C

2: 70 percent / Cs₂CO₃; 18-crown-6 ether / dimethylformamide / 0.17 h / 120 °C / 1500.12 Torr / microwave irradiation

3: 98 percent / NaOMe / methanol / 1 h / 20 °C

With 18-crown-6 ether; sodium methylate; caesium carbonate; palladium dichloride; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo061521t