2-Methoxy-5-nitrotropone

Base Information

Chemical Name:2-Methoxy-5-nitrotropone
CAS No.:14628-90-1
Molecular Formula:C8H7 N O4
Molecular Weight:181.148
Hs Code.:2914700090
European Community (EC) Number:238-670-3
DSSTox Substance ID:DTXSID40163340
Nikkaji Number:J241.332I
Mol file:14628-90-1.mol

Synonyms:2-methoxy-5-nitrotropone

Suppliers and Price of 2-Methoxy-5-nitrotropone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-Methoxy-5-nitrotropone

Chemical Property:

Vapor Pressure:0.000506mmHg at 25°C
Melting Point:232 °C
Boiling Point:313.1°Cat760mmHg
Flash Point:156.4°C
PSA：72.12000
Density:1.31g/cm³
LogP:1.48680
XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:181.03750770
Heavy Atom Count:13
Complexity:333

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=CC1=O)[N+](=O)[O-]

Technology Process of 2-Methoxy-5-nitrotropone

There total 5 articles about 2-Methoxy-5-nitrotropone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 3084-13-7
5-nitrotropolone

: 14628-90-1
2-methoxy-5-nitro-cycloheptatrien-1-one

Guidance literature:: In 1,2-dimethoxyethane; diethyl ether; for 12h;
DOI:10.1039/b617810c

Reference yield:

: 533-75-5
2-hydroxy-2,4,6-cycloheptatrien-1-one

: 14628-90-1
2-methoxy-5-nitro-cycloheptatrien-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 26 percent / nitric acid / H₂O / 0.08 h / cooling

2: 58 percent / 1,2-dimethoxy-ethane; diethyl ether / 12 h

With nitric acid; In 1,2-dimethoxyethane; diethyl ether; water;
DOI:10.1039/b617810c