6-[(N-acetyl-N-benzylamino)methyl]-9-(2,3,5-tri-O-p-toluoyl-β-D-ribofuranosyl)purine

Base Information

• Chemical Name: 6-[(N-acetyl-N-benzylamino)methyl]-9-(2,3,5-tri-O-p-toluoyl-β-D-ribofuranosyl)purine
• CAS No.: 1025504-02-2
• Molecular Formula: C₄₄H₄₁N₅O₈
• Molecular Weight: 767.838

Synonyms:6-[(N-acetyl-N-benzylamino)methyl]-9-(2,3,5-tri-O-p-toluoyl-β-D-ribofuranosyl)purine

Chemical Property of 6-[(N-acetyl-N-benzylamino)methyl]-9-(2,3,5-tri-O-p-toluoyl-β-D-ribofuranosyl)purine

Chemical Property:

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Technology Process of 6-[(N-acetyl-N-benzylamino)methyl]-9-(2,3,5-tri-O-p-toluoyl-β-D-ribofuranosyl)purine

There total 1 articles about 6-[(N-acetyl-N-benzylamino)methyl]-9-(2,3,5-tri-O-p-toluoyl-β-D-ribofuranosyl)purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

6-(methanesulfonyloxymethyl)-9-(2,3,5-tri-O-(p-toluoyl)-β-D-ribofuranosyl)purine (865434-79-3) + acetyl chloride (75-36-5) + benzylamine (100-46-9) → 6-[(N-acetyl-N-benzylamino)methyl]-9-(2,3,5-tri-O-p-toluoyl-β-D-ribofuranosyl)purine (1025504-02-2)

Guidance literature:

6-(methanesulfonyloxymethyl)-9-(2,3,5-tri-O-(p-toluoyl)-β-D-ribofuranosyl)purine; benzylamine; In acetonitrile; for 4h;

acetyl chloride; With triethylamine; In dichloromethane; for 8h; Further stages.;

DOI:10.1016/j.bmc.2007.11.067

Reference yield: 84.0%

6-[(N-acetyl-N-benzylamino)methyl]-9-(2,3,5-tri-O-p-toluoyl-β-D-ribofuranosyl)purine (1025504-02-2) → C20H23N5O5 (1025504-71-5)

Guidance literature:

With ammonium hydroxide; In methanol; at 50 ℃;

DOI:10.1016/j.bmc.2007.11.067

upstream raw materials:

6-(methanesulfonyloxymethyl)-9-(2,3,5-tri-O-(p-toluoyl)-β-D-ribofuranosyl)purine

acetyl chloride

benzylamine

Downstream raw materials:

C₂₀H₂₃N₅O₅

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