diallyl ((S,E)-(propane-1,3-diylbis(oxy))bis(2-((S)-2-(hydroxymethyl)-4-((E)-prop-1-en-1-yl)-2,3-dihydro-1H-pyrrole-1-carbonyl)-4-methoxy-5,1-phenylene))dicarbamate

Base Information

Chemical Name:diallyl ((S,E)-(propane-1,3-diylbis(oxy))bis(2-((S)-2-(hydroxymethyl)-4-((E)-prop-1-en-1-yl)-2,3-dihydro-1H-pyrrole-1-carbonyl)-4-methoxy-5,1-phenylene))dicarbamate
CAS No.:1343407-83-9
Molecular Formula:C₄₃H₅₂N₄O₁₂
Molecular Weight:816.905
Hs Code.:

diallyl ((S,E)-(propane-1,3-diylbis(oxy))bis(2-((S)-2-(hydroxymethyl)-4-((E)-prop-1-en-1-yl)-2,3-dihydro-1H-pyrrole-1-carbonyl)-4-methoxy-5,1-phenylene))dicarbamate

Synonyms:diallyl ((S,E)-(propane-1,3-diylbis(oxy))bis(2-((S)-2-(hydroxymethyl)-4-((E)-prop-1-en-1-yl)-2,3-dihydro-1H-pyrrole-1-carbonyl)-4-methoxy-5,1-phenylene))dicarbamate

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Chemical Property of diallyl ((S,E)-(propane-1,3-diylbis(oxy))bis(2-((S)-2-(hydroxymethyl)-4-((E)-prop-1-en-1-yl)-2,3-dihydro-1H-pyrrole-1-carbonyl)-4-methoxy-5,1-phenylene))dicarbamate

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Technology Process of diallyl ((S,E)-(propane-1,3-diylbis(oxy))bis(2-((S)-2-(hydroxymethyl)-4-((E)-prop-1-en-1-yl)-2,3-dihydro-1H-pyrrole-1-carbonyl)-4-methoxy-5,1-phenylene))dicarbamate

There total 10 articles about diallyl ((S,E)-(propane-1,3-diylbis(oxy))bis(2-((S)-2-(hydroxymethyl)-4-((E)-prop-1-en-1-yl)-2,3-dihydro-1H-pyrrole-1-carbonyl)-4-methoxy-5,1-phenylene))dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1343407-81-7
((2S,2'S,E)-1,1'-(4,4'-(propane-1,3-diylbis(oxy))bis(2-(((allyloxy)carbonyl)amino)-5-methoxybenzoyl))bis(4-((E)-prop-1-en-1-yl)-2,3-dihydro-1H-pyrrole-2,1-diyl))bis(methylene) diacetate

: 1343407-83-9
diallyl ((S,E)-(propane-1,3-diylbis(oxy))bis(2-((S)-2-(hydroxymethyl)-4-((E)-prop-1-en-1-yl)-2,3-dihydro-1H-pyrrole-1-carbonyl)-4-methoxy-5,1-phenylene))dicarbamate

Guidance literature:: With water; potassium carbonate; In methanol; for 1h;

Reference yield:

: 140658-45-3
1',3'-bis(4-carboxy-2-methoxy-5-nitrophenoxy)propane

: 1343407-83-9
diallyl ((S,E)-(propane-1,3-diylbis(oxy))bis(2-((S)-2-(hydroxymethyl)-4-((E)-prop-1-en-1-yl)-2,3-dihydro-1H-pyrrole-1-carbonyl)-4-methoxy-5,1-phenylene))dicarbamate

Guidance literature:: Multi-step reaction with 10 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 16 h / 20 °C

2: triethylamine / dichloromethane / 0.42 h / -40 °C

3: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 0 °C

4: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere

5: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 3 h / 32 °C / Inert atmosphere

6: lithium borohydride / tetrahydrofuran / 1 h / 0 - 20 °C

7: triethylamine / dichloromethane / 0 - 20 °C

8: zinc; formic acid / ethyl acetate; ethanol / 0.5 h / 15 - 33 °C

9: pyridine / dichloromethane / 2 h / -78 °C

10: potassium carbonate; water / methanol / 1 h

With pyridine; 2,6-dimethylpyridine; lithium borohydride; formic acid; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; water; sodium carbonate; potassium carbonate; triethylamine; N,N-dimethyl-formamide; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; toluene; 5: Suzuki Coupling;

Reference yield:

: 1201630-40-1
1,1‘-[[(propane-1,3-diyl)dioxy]bis[(5-methoxy-2-nitro-1,4-phenylene)carbonyl]]bis[(2S,4R)-methyl-4-hydroxypyrrolidine-2-carboxylate]

: 1343407-83-9
diallyl ((S,E)-(propane-1,3-diylbis(oxy))bis(2-((S)-2-(hydroxymethyl)-4-((E)-prop-1-en-1-yl)-2,3-dihydro-1H-pyrrole-1-carbonyl)-4-methoxy-5,1-phenylene))dicarbamate

Guidance literature:: Multi-step reaction with 8 steps

1: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 0 °C

2: 2,6-dimethylpyridine / dichloromethane / 1 h / -45 - 40 °C / Inert atmosphere

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 3 h / 32 °C / Inert atmosphere

4: lithium borohydride / tetrahydrofuran / 1 h / 0 - 20 °C

5: triethylamine / dichloromethane / 0 - 20 °C

6: zinc; formic acid / ethyl acetate; ethanol / 0.5 h / 15 - 33 °C

7: pyridine / dichloromethane / 2 h / -78 °C

8: potassium carbonate; water / methanol / 1 h

With pyridine; 2,6-dimethylpyridine; lithium borohydride; formic acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; water; sodium carbonate; potassium carbonate; triethylamine; zinc; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; toluene; 3: Suzuki Coupling;