ethyl 4-(1-(2,4-dichlorophenyl)-4-ethyl-3-((2-(1-methyl-1H-tetrazol-5-yl)propan-2-yl)carbamoyl)-1H-pyrazol-5-yl)benzoate

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Chemical Name:ethyl 4-(1-(2,4-dichlorophenyl)-4-ethyl-3-((2-(1-methyl-1H-tetrazol-5-yl)propan-2-yl)carbamoyl)-1H-pyrazol-5-yl)benzoate
CAS No.:1331783-61-9
Molecular Formula:C₂₆H₂₇Cl₂N₇O₃
Molecular Weight:556.451
Hs Code.:

Synonyms:ethyl 4-(1-(2,4-dichlorophenyl)-4-ethyl-3-((2-(1-methyl-1H-tetrazol-5-yl)propan-2-yl)carbamoyl)-1H-pyrazol-5-yl)benzoate

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Chemical Property of ethyl 4-(1-(2,4-dichlorophenyl)-4-ethyl-3-((2-(1-methyl-1H-tetrazol-5-yl)propan-2-yl)carbamoyl)-1H-pyrazol-5-yl)benzoate

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Technology Process of ethyl 4-(1-(2,4-dichlorophenyl)-4-ethyl-3-((2-(1-methyl-1H-tetrazol-5-yl)propan-2-yl)carbamoyl)-1H-pyrazol-5-yl)benzoate

There total 4 articles about ethyl 4-(1-(2,4-dichlorophenyl)-4-ethyl-3-((2-(1-methyl-1H-tetrazol-5-yl)propan-2-yl)carbamoyl)-1H-pyrazol-5-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 64-17-5
ethanol

: 1331783-59-5
5-(4-cyanophenyl)-1-(2,4-dichlorophenyl)-4-ethyl-N-(2-(1-methyl-1H-tetrazol-5-yl)propan-2-yl)-1H-pyrazole-3-carboxamide

: 1331783-61-9
ethyl 4-(1-(2,4-dichlorophenyl)-4-ethyl-3-((2-(1-methyl-1H-tetrazol-5-yl)propan-2-yl)carbamoyl)-1H-pyrazol-5-yl)benzoate

Guidance literature:: With hydrogenchloride; at 0 - 20 ℃; for 41h;
DOI:10.1016/j.bmcl.2011.06.017

Reference yield:

: 1265634-50-1
C₁₉H₁₃Cl₂N₃O₂

: 1331783-61-9
ethyl 4-(1-(2,4-dichlorophenyl)-4-ethyl-3-((2-(1-methyl-1H-tetrazol-5-yl)propan-2-yl)carbamoyl)-1H-pyrazol-5-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 10 h / 0 - 20 °C

2: hydrogenchloride / 41 h / 0 - 20 °C

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2011.06.017

Reference yield:

: 1331783-96-0
2-(1-methyl-1H-tetrazol-5-yl)propan-2-amine

: 1331783-61-9
ethyl 4-(1-(2,4-dichlorophenyl)-4-ethyl-3-((2-(1-methyl-1H-tetrazol-5-yl)propan-2-yl)carbamoyl)-1H-pyrazol-5-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 10 h / 0 - 20 °C

2: hydrogenchloride / 41 h / 0 - 20 °C

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2011.06.017