2-iodo-α-methyl-benzenemethanol

Base Information

Chemical Name:2-iodo-α-methyl-benzenemethanol
CAS No.:122752-70-9
Molecular Formula:C₈H₉IO
Molecular Weight:248.063
Hs Code.:

Synonyms:2-iodo-α-methyl-benzenemethanol

Suppliers and Price of 2-iodo-α-methyl-benzenemethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-iodo-α-methyl-benzenemethanol

Chemical Property:

Boiling Point:283.4±23.0 °C(Predicted)
Density:1.739±0.06 g/cm3(Predicted)

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-iodo-α-methyl-benzenemethanol

There total 8 articles about 2-iodo-α-methyl-benzenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 26260-02-6
2-iodobenzaldehyde

: 75-16-1
methylmagnesium bromide

: 122752-70-9
2-iodo-α-methyl-benzenemethanol

Guidance literature:: In diethyl ether; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol301154f

Reference yield: 84.0%

: 5411-56-3
1-(2-bromophenyl)ethanol

: 122752-70-9
2-iodo-α-methyl-benzenemethanol

Guidance literature:: 1-(2-bromophenyl)ethanol; With diisopropylmagnesium; lithium 2-(dimethylamino)ethanolate; In diethyl ether; at -40 - 20 ℃; Inert atmosphere;

With iodine; In tetrahydrofuran; at -20 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.200802488

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 122752-70-9
2-iodo-α-methyl-benzenemethanol

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / diethyl ether / 2 h / Reflux

2: iron(III)-acetylacetonate / diethyl ether / -78 °C / Inert atmosphere

3: Candida tenuis AKR₂B₅ xylose reductase [E_.⁽¹⁾C₁₁₁₇₅]; water; NADH / ethanol / 25 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction

With thionyl chloride; iron(III)-acetylacetonate; Candida tenuis AKR₂B₅ xylose reductase [E_.⁽¹⁾C₁₁₁₇₅]; water; NADH; In diethyl ether; ethanol;
DOI:10.1039/c1ob05510k