C₁₀H₁₁NO₃Se

Base Information

• Chemical Name: C₁₀H₁₁NO₃Se
• CAS No.: 1474030-25-5
• Molecular Formula: C₁₀H₁₁NO₃Se
• Molecular Weight: 272.162
• Mol file: 1474030-25-5.mol

Synonyms:C₁₀H₁₁NO₃Se

Chemical Property of C₁₀H₁₁NO₃Se

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₀H₁₁NO₃Se

There total 2 articles about C₁₀H₁₁NO₃Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(chloroacetyl)glycine (6319-96-6) + sodium phenylselenide (23974-72-3) → C10H11NO3Se (1474030-25-5)

Guidance literature:

In ethanol; water; at 20 ℃; for 2h; pH=Ca. 9; Inert atmosphere; Cooling with ice;

DOI:10.1016/j.jorganchem.2013.07.057

Reference yield:

diphenyl diselenide (1666-13-3) → C10H11NO3Se (1474030-25-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / Inert atmosphere; Cooling with ice

2: water; ethanol / 2 h / 20 °C / pH Ca_. 9 / Inert atmosphere; Cooling with ice

With sodium tetrahydroborate; In ethanol; water;

DOI:10.1016/j.jorganchem.2013.07.057

upstream raw materials:

N-(chloroacetyl)glycine

sodium phenylselenide

diphenyl diselenide

Refernces